Temperature-tunable negative magnetic permeability part based on ferroelectric ceramic grain and its making method
A technology of ferroelectric ceramics and negative magnetic permeability, which is applied in the direction of waveguide devices, electrical components, circuits, etc., and can solve the problems of limited application range, expensive, and complex geometric shapes of metal structural units
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Embodiment 1
[0046] Preparation of Ba by solid-phase reaction synthesis 0.5 Sr 0.5 TiO 3 (BST) powder. The method uses high-purity BaCO 3 , SrCO 3 and TiO 2 As a raw material, react with the following equation to obtain Ba 0.5 Sr 0.5 TiO 3 Powder.
[0047] 0.5BaCO 3 +0.5SrCO 3 +TiO 2 = Ba 0.5 Sr 0.5 TiO 3 +CO 2 ↑
[0048] BaCO 3 , SrCO 3 and TiO 2 Mix according to the above proportions, after ball milling, drying and sieving, calcining at 1150°C for 3 hours, then ball milling and drying to obtain BST powder for use.
[0049] Using the ceramic slurry casting technology, the BST powder prepared above is made into a slurry for casting to obtain a BST casting sheet with a thickness of 0.63mm, and then cut the casting sheet into cubes with a side length of 0.63mm . Then the BST cube was debinding at 400°C, and finally sintered at 1400°C for 3 hours to obtain a BST ceramic cube with a side length of 0.45mm. The measurement results of its temperature and dielectric propertie...
Embodiment 2
[0053] With embodiment one, utilize solid phase reaction synthesis method to prepare Ba 0.5 Sr 0.5 TiO 3 (BST) powder, and the BST ceramic cube whose side length is 0.55mm is obtained by using ceramic slurry casting technology.
[0054] A circular hole array with a diameter of 0.78 mm is drilled on a polytetrafluoroethylene plate with a thickness of 1.25 mm by using a numerical control machine tool. Then, using the polytetrafluoroethylene plate as a template, the ceramic cubes were embedded into the round holes of the polytetrafluoroethylene template to prepare a two-dimensional ceramic cube array. Then align the round holes of the polytetrafluoroethylene plates embedded with ceramic cubes to perform lamination and bonding to obtain a three-dimensional ceramic cube array.
[0055] The above-mentioned three-dimensional BST cube array is placed in a temperature control device to obtain a temperature-tunable isotropic negative magnetic permeability device of ferroelectric cera...
Embodiment 3
[0057] With embodiment one, utilize solid phase reaction synthesis method to prepare Ba 0.4 Sr 0.6 TiO 3 (BST) powder, mix BST powder with 5wt% MgO powder and mix with organic solvent to form a slurry for casting to make a casting sheet with a thickness of 1.25mm, then debinding and sintering to obtain the side length A ceramic cube with a diameter of 1.0mm has a relative permittivity of 1600 at room temperature of 25°C.
[0058] A circular hole array with a diameter of 1.42 mm was drilled on a polytetrafluoroethylene plate with a thickness of 2.5 mm by using a numerical control machine tool. Then, using the polytetrafluoroethylene plate as a template, the ceramic cubes were embedded into the round holes of the polytetrafluoroethylene template to prepare a two-dimensional ceramic cube array. Then align the round holes of the polytetrafluoroethylene plates embedded with ceramic cubes to perform lamination and bonding to obtain a three-dimensional ceramic cube array. The abo...
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