Method for preparing cement additive

A cement additive and cross-linking agent technology, applied in the field of cement additive preparation, can solve problems affecting cementing quality, cross-channeling between layers, low-pressure layer pollution, etc., to improve cementing quality, prevent annular air channeling, and increase strength Effect

Active Publication Date: 2009-11-04
ANTON OILFIELD SERVICES (GRP) LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] In view of shallow depth of reservoir, high oil-gas ratio, a large amount of natural gas dissolved in underground crude oil, low viscosity and low density of crude oil, when the oil layer is opened, when the pressure drops below the saturation pressure, the crude oil in the formation will be seriously degassed. During the process, the released gas escapes into the cement stone matrix, or enters the gap between the cement and the casing or the cement and the well wall, causing interlayer interleaving or even entering the wellhead, which eventually leads to low cement cement bond strength or interlayer channeling , which seriously affects the quality of cementing. Even if remedial measures such as cement squeezing are adopted, it is difficult to be effective, and it will have adverse effects on subsequent oilfield operations such as water injection, acid fracturing, and layered mining, and even cannot be carried out.
In addition, due to the large difference between the oil layers, the high-pressure layer and the low-pressure layer exist at the same time. If the density of the cement slurry is increased to prevent gas channeling, it will cause pollution to the low-pressure layer, or even pressure leakage. Gas channeling affects the quality of cementing. In severe cases, formation oil, gas and water may channel to the surface

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0012] 4% (weight) of acrylamide, 3% organic boron, 1% sodium hydroxide, 2.5% silicon powder and water are cross-linked and polymerized at 75°C to form a gel, which is then dried, crushed and sieved to prepare A cement additive with a particle size of 0.5-0.9 mm is obtained.

[0013] The above cement additives are added to the cement slurry, and 1.5 parts of cement additives are added to 100 parts (by weight) of the cement slurry. After the cement additive of this embodiment is used, the gas-proof effect is good, and the cementing quality is guaranteed. The cementing quality is qualified The rate reached 94%.

Embodiment 2

[0015] 5% (weight) of acrylamide, 2% borax, 2% sodium hydroxide, 4% silicon powder and water are cross-linked and polymerized at 80°C to form a gel, which is then dried, crushed and sieved to obtain A cement additive with a particle size of 0.5-0.9mm.

[0016] The above cement additives are added to the cement slurry, and 2 parts of cement additives are added to 100 parts (weight) of cement slurry. After the cement additive of this embodiment is adopted, the gas-proof effect is good, and the cementing quality is guaranteed, and the cementing quality is qualified The rate reached 97%.

Embodiment 3

[0018] 8% (weight) of acrylamide, 4% organic boron, 3.5% potassium hydroxide, 1% fly ash and water are cross-linked and polymerized at 90°C to form a gel, which is then dried, crushed and sieved. A cement additive with a particle size of 0.5-0.9 mm is obtained.

[0019] The above-mentioned cement additives are added to the cement slurry, and 3 parts of cement additives are added to 100 parts (weight) of cement slurry. After the cement additive of this embodiment is adopted, the gas-proof effect is good, and the quality of cementing is guaranteed, and the quality of cementing is qualified. The rate reached 95%.

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Abstract

The invention discloses a preparation method of a cement additive, which comprises the following steps: a) adding 4-8% by weight of acrylamide, 2-4% by weight of a crosslinking agent, 1-3.5% by weight of an initiator, 1- 4% by weight of the reinforcing agent and the rest of the water are cross-linked and polymerized under normal pressure to form a gel; b) drying and pulverizing the above-mentioned gel to obtain a cement additive. The cement additive prepared by the method of the invention is applied to the cement system of oil field cementing, which can prevent gas channeling, improve the cementing quality, and the qualified rate of the cementing quality is increased from the original 45% to more than 94%.

Description

technical field [0001] The invention relates to a preparation method of a cement additive, in particular to a preparation method of a cement additive used for oil field cementing. Background technique [0002] In view of shallow depth of reservoir, high oil-gas ratio, a large amount of natural gas dissolved in underground crude oil, low viscosity and low density of crude oil, when the oil layer is opened, when the pressure drops below the saturation pressure, the crude oil in the formation will be seriously degassed. During the process, the released gas escapes into the cement stone matrix, or enters the gap between the cement and the casing or the cement and the well wall, causing interlayer interleaving or even entering the wellhead, which eventually leads to low cement cement bond strength or interlayer channeling , Seriously affecting the quality of cementing, even if remedial measures such as cement extrusion are adopted, it is difficult to be effective, and it will adv...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B7/42C04B24/26
Inventor 张世甫吴锦平
Owner ANTON OILFIELD SERVICES (GRP) LTD
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