Firming agent for surface layer of coal
A curing agent and surface technology, applied in chemical instruments and methods, other chemical processes, loading/unloading, etc., can solve problems such as physical health hazards, passenger health threats, time-consuming and labor-consuming, and achieve the effect of avoiding dust pollution
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Embodiment 1
[0027] Raw material ratio:
[0028] Raw material name Proportion (wt%) Raw material name Proportion (wt%)
[0029] Polyvinyl alcohol 0.5 Potassium permanganate solution (concentration is 1wt%) 0.4
[0030] Starch 4 Borax or boric acid solution (concentration is 5wt%) 2
[0031] Caustic soda solution (concentration is 10wt%) 4 water 99.1
[0032] Operation process:
[0033] As shown in Figure 1, according to the proportion of raw materials, add 50% of the total water into the reaction kettle, then add 0.5% polyvinyl alcohol, stir, heat up to 99°C to completely dissolve the polyvinyl alcohol, cool down to 60°C, add 4% corn starch, stirred and kept warm for 1 hour to carry out graft modification; after modification, cool the material to 35°C, then add 0.3% potassium permanganate solution, oxidize for 1 hour, watch the color of the solution, it gradually changes from purple to colorless ; Then, under the condition of stirring, slowly add 4% caustic soda solution in the reactio...
Embodiment 2
[0035] Raw material ratio:
[0036] Raw material name Proportion (wt%) Raw material name Proportion (wt%)
[0037]Polyvinyl alcohol 1.5 Potassium permanganate solution (concentration is 1wt%) 0.6
[0038] Starch 6 Borax or boric acid solution (concentration is 5wt%) 5
[0039] Caustic soda solution (concentration is 10wt%) 8 water 78.9
[0040] Operation process:
[0041] As shown in Figure 1, according to the proportion of raw materials, add 50% of the total water into the reactor, then add 1.5% polyvinyl alcohol, stir, heat up to 99°C to completely dissolve the polyvinyl alcohol, cool down to 60°C, add Corn starch 6%, stirring and keeping warm for 1 hour for graft modification; after modification, cool the material to 35°C, then add 0.6% potassium permanganate solution, oxidize for 1 hour, watch the color of the solution, gradually change from purple to colorless ; Then, under the condition of stirring, slowly add 8% caustic soda solution in the reaction kettle, the mate...
Embodiment 3
[0043] Raw material ratio:
[0044] Raw material name Proportion (wt%) Raw material name Proportion (wt%)
[0045] Polyvinyl alcohol 1 Potassium permanganate solution (concentration is 1wt%) 0.4
[0046] Starch 5 Borax or boric acid solution (concentration is 5wt%) 3
[0047] Caustic soda solution (concentration is 10wt%) 6 water 84.6
[0048] Operation process:
[0049] As shown in Figure 1, according to the proportion of raw materials, add 50% of the total water into the reactor, then add 1% polyvinyl alcohol, stir, heat up to 99°C to completely dissolve the polyvinyl alcohol, cool down to 60°C, add 5% corn starch, stirring and keeping warm for 1 hour to carry out graft modification; after modification, cool the material to 35°C, then add 0.5% potassium permanganate solution, oxidize for 1 hour, watch the color of the solution, gradually change from purple to colorless Then, under stirring, slowly add 6% caustic soda solution in the reaction kettle, the material becomes ...
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