Adding substance for reducing furnace tube deposition coking and improving liquid yield of delayed coker
A technology of delayed coking and additives, applied in cracking, non-catalytic thermal cracking, treatment equipment corrosion/fouling inhibition, etc. It can solve the problems of lack of ashless non-metallic dispersant and unsatisfactory effect, so as to increase liquid recovery and improve Yield effect
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Embodiment 1
[0030] Mix 9kg of monoethanolamine and 3kg of vegetable oleic acid, heat up to 170°C, and keep stirring, the reaction water is taken out with toluene, when no more reaction water is produced, stop the reaction, evaporate the toluene, and cool naturally to normal pressure , That is, ashless non-metallic dispersant. Then mix 5kg of ashless non-metallic dispersant, 20kg of thermal cracking initiator, 25kg of chemical reaction inhibitor, 30kg of anti-scorch agent and 5kg of solvent, and stir at 90°C for 1.5 hours. Then it is cooled to normal temperature and sent to filter to remove solid impurities to obtain the finished additive to be prepared.
Embodiment 2
[0032] Mix 9kg of triethanolamine and 3kg of vegetable oleic acid, heat up to 170°C, and keep stirring, the reaction water is taken out with toluene, when no more reaction water is produced, stop the reaction, evaporate the toluene, and cool naturally to normal pressure , That is, ashless non-metallic dispersant. Then mix 5kg of ashless non-metallic dispersant, 20kg of thermal cracking initiator, 25kg of chemical reaction inhibitor, 30kg of anti-scorch agent and 5kg of solvent, and stir at 90°C for 1.5 hours. Then it is cooled to normal temperature and sent to filter to remove solid impurities to obtain the finished additive to be prepared.
Embodiment 3
[0034] a. Evaluation method of scale and coke reduction effects of additives, the test device is shown in Figure 1.
[0035] b. Main instruments and equipment are shown in Table 1
[0036] Table 1 Main instruments and equipment of scale reduction and coke reduction test device
[0037] serial number
name
Model / Specification
place of origin
1
2
3
4
Heating furnace tube
Tubular temperature controlled heating furnace
Inner diameter 150, height 400 stainless steel
Cylindrical container
J-W 0.5 / 32
4mm inner diameter stainless steel pipe
Temperature control 300±5℃, read
Number accuracy 0.1°C
self made
Hangzhou Zhijiang Petrochemical Co., Ltd.
equipment co., ltd.
self made
self made
[0038] 5
6
7
cooling condenser
Coker Light Oil Receiver
pressure gaug...
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Abstract
Description
Claims
Application Information
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