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Device and method for co-production or single production of refined methanol with rough methanol

A production device and technology for crude methanol, applied in chemical instruments and methods, ether preparation, organic compound preparation, etc., can solve the problems of inflexible production plans for refined methanol and dimethyl ether products, and achieve flexible product plans and improve equipment. Utilization, strong effect

Inactive Publication Date: 2008-05-07
褚雅志
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0011] The purpose of the present invention is to provide a production device for co-production of crude methanol or single production of refined methanol and / or dimethyl ether against the inflexible production scheme of refined methanol and dimethyl ether in the prior art, so as to save the device Purpose of investment and flexible adjustment of production plan

Method used

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  • Device and method for co-production or single production of refined methanol with rough methanol
  • Device and method for co-production or single production of refined methanol with rough methanol
  • Device and method for co-production or single production of refined methanol with rough methanol

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Embodiment Construction

[0021] Referring to Fig. 1, it comprises a reactor R1, a tower T1, two towers T2, three towers T3 and four towers T4, said each tower has a tower top condenser and a tower still reboiler, wherein the tower top condenses The existing primary condenser or secondary condenser can be used as the condenser. To simplify the description, the structure of the primary condenser is shown in the figure. In the project, some pumps and tanks need to be added to this device, which is common knowledge in this industry, and it is omitted in this figure for the sake of simplification.

[0022] The specific connections between the reactor R1 and the four towers are as follows:

[0023] 1. The crude methanol raw material is connected to the feed port of the first tower T1 through three heat exchangers E1, E2 or E2 across the line, E8, and the heat exchangers E1 and E2 are respectively used for the crude methanol feed and the bottom of the three tower T3 The product exchanges heat with the top p...

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Abstract

The invention relates to a production device and method for co-production of crude methanol or single production of refined methanol and / or dimethyl ether. It includes a reactor and four towers. The present invention organically combines the methanol rectification device and the dimethyl ether device, and all the rectification towers of dimethyl ether are shared with the methanol rectification tower, which can realize the co-production of refined methanol and dimethyl ether or the single production of refined methanol or dimethyl ether The operation of the three technical processes of methyl ether saves investment and energy, reduces production costs, makes the best use of everything, and improves the utilization rate of the device. Moreover, when co-producing or producing dimethyl ether alone, the crude methanol raw material passes through the first tower to remove light components, which reduces the load on the reactor, the reaction product is easy to separate, and the quality of the dimethyl ether product is high; The methanol vapor returns directly to the three towers without condensation, and the separation capacity of the three towers is used to obtain refined methanol, which saves investment and reduces energy consumption.

Description

Technical field [0001] The invention relates to a device and method for producing refined methanol and dimethyl ether in the field of chemical industry, in particular, it is a production device and method for co-production of crude methanol or single production of refined methanol and / or dimethyl ether. Background technique [0002] Methanol and dimethyl ether are the two most common products of coal-to-oil at present, and their raw materials are crude methanol. The typical composition of crude methanol is as follows: [0003] components Contentwt% hydrogen 10±5ppm Nitrogen 70±30ppm carbon monoxide 100±50ppm carbon dioxide 0.9±0.3 methane 200±100ppm ethane 50±30ppm Dimethyl ether 0.15±0.1 Methyl formate 0.10±0.5 water 13±10 acetone 50±40ppm Methanol 85±10 ethanol 0.15±0.1 propanol 300±100ppm Butanol 100±50ppm ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C07C29/80C07C31/04C07C41/09C07C43/04B01D3/02
Inventor 褚雅志王胜利杨忠绪
Owner 褚雅志
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