Composite plating process and equipment for magnetron sputtering-laser heating

A magnetron sputtering and laser heating technology, applied in sputtering coating, metal material coating process, ion implantation coating and other directions, can solve the problems of grain growth, poor bonding strength of film base, long time, etc. Achieve the effect of high power and high density thermal energy

Inactive Publication Date: 2008-06-11
GUILIN UNIV OF ELECTRONIC TECH
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  • Abstract
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Problems solved by technology

Among the above equipment and process methods, except for the double-layer glow ionized metal infiltration equipment and technology, the rest of the equipment and process technologies all form a deposition coating on the surface of the material without a diffusion layer.
Therefore, the bonding strength of the film base is poor, and it is easy to peel off
The double-layer glow ionization metallization equipment and technology adopts the diode-type glow discharge sputtering to provide the alloying elements to be infiltrated. Due to the low ionization rate, the number of alloying elements to be infiltrated per unit time is limited, making the surface metallization process affected
In addition, when the double-layer glow ion infiltrates the metal, the infiltrated workpiece is heated by ion bombardment, the heating speed is slow, the time is long, and the grain grows seriously.
The diffusion of alloy atoms to be infiltrated is mainly intragranular diffusion, and the diffusion speed is very low

Method used

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  • Composite plating process and equipment for magnetron sputtering-laser heating

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Embodiment Construction

[0023] The present invention will be described in further detail below in conjunction with the accompanying drawings.

[0024] The size is 100mm * 100mm * 5mm, and the infiltrated workpiece 3 made of 20 steel is placed on the brackets of the longitudinal reciprocating mechanism 6 and the transverse reciprocating mechanism 7, and the size is selected to be φ100mm * 5mm (diameter * high) magnetic The magnetron sputtering target 1 is arranged above the workpiece to be infiltrated. The magnetron sputtering target is made of pure metal Mo, and the vacuum is evacuated to an ultimate vacuum degree of 3×10 -3 Above pa, fill the gas medium with argon gas to the working vacuum degree of 10Pa, first apply a high voltage DC voltage -500V to the magnetron sputtering target 1, and ion sputter the target for 20 minutes, stop sputtering, turn on the transverse reciprocating mechanism 7, and simultaneously laser The heating device 5 scans and heats the surface of the infiltrated workpiece 3 at...

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Abstract

The invention discloses the magnetron sputtering-laser heating composite diffusion coating technology and the equipment, by utilizing the magnetron sputtering and a laser heating device, a single diffusion coating layer or a composite diffusion coating layer with a diffusion layer and a sedimentary layer or the diffusion layer plus the sedimentary layer which comprises metal element and nonmetal element is formed on the surface of a conducting workpiece. The invention has the advantages that by utility a magnetron sputtering target, sufficient pre-diffusing alloy element can be provided; by utilizing the laser heating, the diffused material can heated to high temperature in a short time and the diffusing speed is greatly increased; the DEG Cree of vacuum of the metal for diffusing is increased at least one order of magnitude compared with the common alloying method, and the surface quality of the diffused workpiece can be greatly improved; the diffusion coating can be performed continuously, and the production in large area and large scale can be realized.

Description

Technical field: [0001] The invention relates to plasma surface metallurgy, in particular to a magnetron sputtering-laser heating composite diafiltration process and equipment capable of forming an alloy layer on the surface of a conductive material. Background technique: [0002] At present, various equipment and processes for plasma surface modification using gas discharge mainly include: double-layer glow ion plating metal plating equipment and technology, multi-arc ion plating equipment and technology, magnetron sputtering ion plating equipment and technology, DC two-pole sputtering, DC three-pole or four-pole sputtering plating equipment and technology, etc. Among the above equipment and process methods, except for the double-layer glow ion infiltration metallization equipment and technology, the rest of the equipment and process technologies all form a deposited coating on the surface of the material without a diffusion layer. Therefore, the bonding strength of the fi...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C23C14/35C23C14/54C23C14/58
Inventor 高原徐晋勇高清郑英唐光辉程东
Owner GUILIN UNIV OF ELECTRONIC TECH
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