Method for manufacturing acrylic ester emulsion containing phosphate group for antiseptic paint
A phosphate group, anti-corrosion coating technology, applied in anti-corrosion coatings, coatings and other directions, can solve the problems of many side reactions, inconvenient use, unsatisfactory drying speed, etc., to achieve accelerated drying speed, convenient use, excellent anti-corrosion effect of function
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Embodiment 1
[0021] Embodiment 1: the component of emulsion and parts by weight thereof (unit is gram) are as follows:
[0022] Methyl methacrylate 100
[0023] Butyl acrylate 127.5
[0024] PAM-100 22.5
[0025] Sodium dodecylbenzenesulfonate 10
[0026] Ammonium persulfate 1.0
[0027] Deionized water 262.5
[0028] Process flow: Mix methyl methacrylate, butyl acrylate, and PAM-100 evenly to form polymerized monomers and set aside → then add 225 grams of deionized water and dodecane to a reaction vessel equipped with a thermometer, stirring, and reflux device 10 grams of sodium phenylsulfonate, start stirring and heat up to 70-90°C → then add 30 grams of polymerized monomers and 0.4 grams of ammonium persulfate to the reaction vessel, and keep warm at 70-90°C for 45 minutes → After the heat preservation is completed, Dissolve the remaining ammonium persulfate in 37.5 grams of deionized water, and add them into the reaction vessel evenly with the remaining polymerized monomers within...
Embodiment 2
[0029] Embodiment 2: the component of emulsion and parts by weight thereof (unit is gram) are as follows:
[0030] Methyl methacrylate 100
[0031] Butyl acrylate 100
[0032] PAM-100 50
[0033] Sodium dodecylbenzenesulfonate 10
[0034] Ammonium persulfate 1.0
[0035] Deionized water 262.5
[0036] Process flow: Mix methyl methacrylate, butyl acrylate, and PAM-100 evenly to form polymerized monomers and set aside → then add 225 grams of deionized water and dodecane to a reaction vessel equipped with a thermometer, stirring, and reflux device 10 grams of sodium phenylsulfonate, start stirring and heat up to 70-90°C, add 30 grams of polymerized monomers and 0.4 grams of ammonium persulfate, and keep warm at 70-90°C for 45 minutes → After the heat preservation is completed, the remaining persulfuric acid Dissolve ammonium in 37.5 grams of deionized water, and add the remaining polymerized monomers into the reaction vessel evenly within 2 to 3 hours. After the addition, th...
Embodiment 3
[0037] Embodiment 3: the component of emulsion and parts by weight thereof (unit is gram) are as follows:
[0038] Methyl methacrylate 120
[0039] Butyl acrylate 127.5
[0040] PAM-100 2.5
[0041] Sodium dodecylbenzenesulfonate 10
[0042] Ammonium persulfate 1.0
[0043] Deionized water 262.5
[0044] Process flow: Mix methyl methacrylate, butyl acrylate, and PAM-100 evenly to form a polymerized monomer and reserve → then add 225 grams of deionized water and dodecane to a reaction vessel equipped with a thermometer, stirring, and reflux device 10 grams of sodium phenylsulfonate, start stirring and heat up to 70-90°C, then add 30 grams of polymerized monomers and 0.4 grams of ammonium persulfate, and keep warm at 70-90°C for 45 minutes → After the heat preservation is completed, put the remaining persulfate Ammonium sulfate is dissolved in 37.5 grams of deionized water, and is evenly added to the reaction vessel with the remaining polymerized monomers in 2 to 3 hours. A...
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