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Method of manufacturing gradual-change bore diameter stainless steel antipriming pipe

A technology of stainless steel and porous tubes, applied in separation methods, chemical instruments and methods, filtration and separation, etc., can solve the problems of increasing the manufacturing cost of metal porous materials, not stating the performance, unfavorable for large-scale and wide application, etc., to achieve the improvement of demoulding success efficiency, ensure filtration accuracy, and improve the effect of air permeability coefficient

Active Publication Date: 2009-05-13
NORTHWEST INSTITUTE FOR NON-FERROUS METAL RESEARCH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Sudden change (also known as step shape - with obvious material interface) pore size gradient porous material is a filter control layer or transition layer attached to the support of the previous layer of large pores, because the particle diameter of the powder is mutated, the next layer The particles will block the upper layer of large pores, thereby reducing the permeability of the porous material, and the multiple molding and sintering processes used will increase the manufacturing cost of the metal porous material. These disadvantages are not conducive to its large-scale and wide application.
[0005] The invention patent with the application number of 200510033633.3 "Porous non-layer boundary gradient metal film tube and its preparation method" introduces a preparation method of a porous non-interface gradient metal film tube, but does not state the specific properties of the corresponding powder corresponding material; in addition, the The preparation method of the metal porous tube described in the patent has some disadvantages: for example, after the metal porous tube is formed, the green body of the porous tube is not easy to demould, and the thickness of the metal porous tube is not easy to control, etc.

Method used

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  • Method of manufacturing gradual-change bore diameter stainless steel antipriming pipe
  • Method of manufacturing gradual-change bore diameter stainless steel antipriming pipe
  • Method of manufacturing gradual-change bore diameter stainless steel antipriming pipe

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036] Take the irregular shape stainless steel (304L) powder A (such as image 3Shown), mix with the polyvinyl alcohol solution that mass percent concentration is 10%, the solid content of the powder suspension that obtains after mixing is 20% (mass percentage), adds getter in the powder suspension and removes the polyvinyl alcohol in the powder suspension Gas, after stirring evenly, pour it into the two-half split rigid tube mold, and put it on the centrifuge for centrifugation; the speed of the centrifuge is adjusted from 0 to 3000 rpm, and the centrifugation time is 15 minutes; Half-type bisecting rigid tube mold, pour out the clear liquid in the mold, dry the stainless steel porous tube with gradient aperture and demould; sinter the porous tube in a vacuum furnace; finally use the FBP-I porous material tester to test The prepared gradient aperture stainless steel porous tube has a maximum pore diameter of 43 μm and a relative air permeability of 540 m 3 / m 2 ·KPa·h.

Embodiment 2

[0038] Take the irregular shape stainless steel (304L) powder B (such as image 3 Shown), mix with the polyvinyl alcohol solution that mass percent concentration is 5%, the solid content of the powder suspension that obtains after mixing is 10% (mass percentage), adds getter in the powder suspension and removes in the powder suspension Gas, after stirring evenly, pour it into the two-half split rigid tube mold, and put it on the centrifuge for centrifugation; the speed of the centrifuge is adjusted from 0 to 3000 rpm, and the centrifugation time is 15 minutes; Half-type bisecting rigid tube mold, pour out the clear liquid in the mold, dry the stainless steel porous tube with gradient aperture and demould; sinter the porous tube in a vacuum furnace; finally use the FBP-I porous material tester to test The prepared gradient aperture stainless steel porous tube has a maximum pore diameter of 21 μm and a relative air permeability of 417m 3 / m 2 ·KPa·h.

Embodiment 3

[0040] Weigh the irregular shape stainless steel (304L) powder C (such as image 3 Shown), mix with the polyvinyl alcohol solution that mass percent concentration is 8%, the solid content of the powder suspension that obtains after mixing is 16% (mass percentage), adds getter in the powder suspension and removes the polyvinyl alcohol in the powder suspension Gas, after stirring evenly, pour it into the two-half split rigid tube mold, and put it on the centrifuge for centrifugation; the speed of the centrifuge is adjusted from 0 to 3000 rpm, and the centrifugation time is 15 minutes; Half-type bisecting rigid tube mold, pour out the clear liquid in the mold, dry the stainless steel porous tube with gradient aperture and demould; sinter the porous tube in a vacuum furnace; finally use the FBP-I porous material tester to test The maximum pore diameter of the prepared gradient aperture stainless steel porous tube is 31 μm, and the relative air permeability coefficient is 444m 3 / ...

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Abstract

The invention provides a preparation method for a stainless steel perforated pipe with gradually-varied aperture, the invention adopts the preparation process that stainless steel powder is mixed with a certain polyvinyl alcohol solution to prepare stainless steel powder suspension, and getter is added into the suspension and poured into a two-piece-type opening and closing rigid pipe die made of stainless steel after even stirring, which centrifugally takes shape on a centrifuge, thereby preparing a green body of the stainless steel perforated pipe with gradually-varied aperture grads; the green body is dried in a blast-type baking oven, and then the demoulding is performed; the green body of the stainless steel perforated pipe after drying is sintered in a vacuum stove, the sintering atmosphere adopts vacuum, and the stainless steel perforated pipe with gradually-varied aperture grads is prepared after cooling. The invention has the advantages that the demoulding attainment rate of the green body of the stainless steel perforated pipe with gradually-varied aperture is greatly enhanced, and the filtering precision of the perforated pipe is ensured; meanwhile, the air transmission coefficient of the stainless steel perforated pipe with gradually-varied aperture is enhanced, and the preparation method solves the phenomenon of the reciprocal relationship between the filtering precision of the stainless steel perforated pipe and the transmission performance in the filtration, separation and application process.

Description

technical field [0001] The invention relates to a method for preparing a metal porous pipe, in particular to a method for preparing a stainless steel porous pipe with variable apertures. Background technique [0002] At present, most porous metal filter materials are based on uniform porous metal materials, and one or more layers of porous membranes are coated on the surface to improve the filtration accuracy. With the rapid development of industry, the requirements for filter materials are getting higher and higher. As the matrix of the filter membrane layer, uniform porous materials can no longer meet the requirements of large air permeability and high precision in some departments. [0003] Metallic porous materials are a class of metal materials with obvious pore characteristics (porosity can reach up to 98%). In terms of the use environment, compared with organic and ceramic porous materials, it mainly has three advantages: high mechanical strength, good thermal conduc...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B22F5/12B01D39/20
Inventor 奚正平汤慧萍刘忠军汪强兵
Owner NORTHWEST INSTITUTE FOR NON-FERROUS METAL RESEARCH
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