Accelerant for textile dyeing, preparation method and applications thereof
A technology for textile printing and dyeing and dye accelerator, applied in the field of textile printing and dyeing, can solve the problems of inability to popularize and apply, too expensive, etc., and achieve the effects of saving printing and dyeing water, reducing production costs, and reducing salt pollution
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Embodiment 1
[0038] (1) Use 10g of neodymium oxide and yttrium oxide with a purity of more than 99.9% as a rare earth source, dissolve them in 100ml 2mol / L hydrochloric acid to obtain a rare earth chloride solution, heat the rare earth chloride solution to 80°C, and add 50g of A 5% aqueous solution of the mixture of diethylenetriaminepentaacetic acid (DTPA) was incubated at 80°C for 3 hours to generate a rare earth organic acid complex;
[0039] (2) Fully mix 15g of 2,4,6 trichlorophenol with 1g of modifier A (non-ionic fluorocarbon surfactant, produced by Dow Chemical Company), and add the reacted rare earth organic acid complex in step (1). After reacting at 60°C for 1 hour, add a small amount of 2g of leveling agent B (styrene phenol polyoxyethylene ether ammonium sulfate), and add distilled water to 500ml, fully stir for 30min and then discharge, that is Get the final product liquid environmental protection dye accelerator XK08A. Its fastness index and quality index are shown in Table...
Embodiment 2
[0041] Replace the rare earth source neodymium oxide and yttrium oxide in Example 1 with mixed rare earth oxides (purity > 85%), and replace the complexing agent with citric acid (CA). Accelerator XK08B. Its fastness index and quality index are shown in Table 1.
Embodiment 3
[0043] The rare earth source neodymium oxide and yttrium oxide in Example 1 were replaced with yttrium chloride and selenium chloride, and the complexing agent was replaced with fumaric acid. Other operations were the same as in Example 1, and the required dyeing accelerator was obtained.
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