Method for preparing sodium copper chlorophyllin by using watermelon outer peel
A technology for sodium copper chlorophyll and chlorophyll, applied in copper organic compounds, organic chemistry and other directions, can solve the problems of low chlorophyll extraction efficiency, large solvent loss, chlorophyll damage, etc., and achieve the effects of avoiding large losses, avoiding degradation and convenient operation.
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[0030] (1) First clean the skin of fresh watermelon, cut off the skin with a thickness of 2mm, crush it with a pulverizer, and then use a vacuum freeze dryer to pre-freeze it at minus 40°C for 4 hours, and then freeze the intermediate at minus 15°C Freeze-dry for 24 hours, heat up to 20°C and dry for 4 hours. During the whole freeze-drying process, the vacuum degree in the warehouse is maintained at about 110Pa (the specific vacuum freeze dryer can be Zhengzhou Zhongfa Vacuum Equipment Co., Ltd., ZLGS series food vacuum freeze-drying equipment). (2) Take 1000 grams of frozen watermelon epidermis powder, thaw at room temperature, add acetone:ethanol=1:1 (V / V) mixed solvent according to 1:8 solid-liquid ratio after thawing, after mixing, room temperature intermittent ultrasonic extraction two times (ultrasonic power: 100W, ultrasonic frequency: 28kHz), 30min each time. (3) The extract was filtered, and the filtrate was evaporated to dryness in vacuo at 55° C. to obtain crude ch...
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