Method for preparing magnesium peroxide by non-emulsion process
A magnesium peroxide, non-emulsifying technology, applied in chemical instruments and methods, peroxide/peroxyhydrate/peroxyacid/superoxide/ozonide, inorganic chemistry, etc., can solve the problem of high cost, peroxide Low magnesium content and other issues, to achieve the effect of convenient operation, reduce raw material cost, and facilitate large-scale industrial production
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Embodiment 1
[0018] Example 1: Add 36 mL of hydrogen peroxide with a mass concentration of 30% in a 500 mL beaker; weigh 0.5 g of hydroxyethylidene diphosphonic acid and add it to the beaker, stir to dissolve it; then add 1.1 mol / L of hydrogen peroxide into the beaker Magnesium chloride solution 150mL, after mixing evenly, add 110mL ammonia solution with a mass concentration of 25% drop by drop under stirring condition; control the temperature of the reaction system at 15±5°C, and stir for 4 hours. Obtain wet product magnesium peroxide by suction filtration after the reaction, wet product magnesium peroxide is after washing, and temperature is 70 ℃, pressure is that vacuum drying under 80mmHg, obtains the powder product that 10g magnesium peroxide content is 47.6%.
Embodiment 2
[0019] Example 2: Add 54mL of hydrogen peroxide with a mass concentration of 20% in a 500mL beaker; weigh 0.5g sodium hydroxyethylidene diphosphonate and add it, stir to dissolve it; then add 1.1mol / L of hydrogen peroxide into the beaker Magnesium chloride solution 150mL, after mixing evenly, add 110mL ammonia solution with a mass concentration of 25% dropwise under stirring; control the temperature of the reaction system at 15±5°C, and stir for 4 hours. Obtain wet product magnesium peroxide by suction filtration after the reaction, wet product magnesium peroxide is after washing, and temperature is 70 ℃, pressure is that vacuum drying under 80mmHg, obtains the powder product that 10.5g magnesium peroxide content is 47.3%.
Embodiment 3
[0020] Example 3: Add 36mL of hydrogen peroxide with a mass concentration of 30% in a 500mL beaker, weigh 0.5g of aminotrimethylene phosphonic acid and add it, stir to dissolve it; then add magnesium sulfate with a concentration of 1.1mol / L to the beaker Solution 150mL, after mixing evenly, add 100mL of sodium hydroxide solution with a mass concentration of 28% drop by drop under stirring; control the temperature of the reaction system at 15±5°C, and stir for 4 hours. Obtain wet product magnesium peroxide by suction filtration after the reaction, wet product magnesium peroxide is after washing, and temperature is 70 ℃, pressure is that vacuum drying under 80mmHg, obtains the powder product that 10.5g magnesium peroxide content is 47.5%.
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