Method for refrigerating, vacuum-drying and purifying ganoderma spore powder
A technology of freeze vacuum drying and Ganoderma lucidum spore powder, which is applied in the direction of pharmaceutical formulas, medical preparations containing active ingredients, plant/algae/fungus/moss ingredients, etc., which can solve allergic reactions, difficult to control the temperature of materials accurately, and excessive dust to avoid human immune response, improve purity and cleanliness, and reduce the number of broken walls
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Embodiment 1
[0038] (1) Weigh 40kg of Ganoderma lucidum spore powder raw material, add 120kg of purified water to the washing container, slowly add Ganoderma lucidum spore powder, and stir with a fast stirrer until it dissolves evenly;
[0039] (2) After removing the stirrer, let it stand for 30min, filter the floating matter in the upper layer, filter the spore powder suspension with 300 mesh silk cloth, discard the bottom layer, and obtain the filtrate;
[0040] (3) The filtrate is press-filtered with an air filter, the filter cake is crushed with a 30-mesh screen of a swing-type granulator, and purified water is added to make up the liquid until the total weight is 128kg, and the mixture is evenly stirred to obtain a mixed solution;
[0041](4) Distribute the mixed solution into freeze-drying trays, evacuate to 60Pa, fill with nitrogen to atmospheric pressure, pre-cool the material to -20°C, pre-cool to -35°C in the back box, and keep for 0.5 hours; evacuate to 15Pa, Heat and sublimate ...
Embodiment 2
[0046] Investigation of the quality of Ganoderma lucidum spore powder by freeze-vacuum drying method and sunlight drying method of Ganoderma lucidum spore powder according to the present invention
[0047] Weigh 40kg of Ganoderma lucidum spore powder raw material, add 130kg of purified water into the washing container, slowly add Ganoderma lucidum spore powder, stir with a fast stirrer until it dissolves evenly; Filter the spore powder suspension with mesh cotton cloth, discard the bottom layer, and obtain the filtrate; filter the filtrate with an air filter, crush the filter cake with a 30-mesh sieve of a swinging granulator, add purified water to prepare the liquid, and filter through the hydraulic pressure Break it into pieces, add purified water to mix up to a total of 130kg, stir evenly to obtain a mixed solution; divide the mixed solution into a freeze-drying tray, vacuumize to 40Pa, fill with nitrogen to atmospheric pressure, pre-cool the material to 0°C, and put it in t...
Embodiment 3
[0051] Investigation of the quality of Ganoderma lucidum spore powder by freeze vacuum drying method and hot air circulation oven drying method of the present invention
[0052] Weigh 40kg of Ganoderma lucidum spore powder raw material; add 133kg of purified water to the washing container, slowly add Ganoderma lucidum spore powder, stir with a fast stirrer until it dissolves uniformly; Filter the spore powder suspension with 300 mesh gauze, discard the bottom layer, and obtain the filtrate; filter the filtrate with an air filter, crush the filter cake with a 30 mesh screen of a swinging granulator, add purified water to make up a total of 133kg , stir evenly to obtain a mixed solution; divide the mixed solution into a freeze-drying tray, vacuumize to 20Pa, fill with nitrogen to atmospheric pressure, pre-cool the material to -15°C, pre-cool the rear box to -35°C, and keep for 4 hours; Vacuum to 1Pa, heat and sublimate to 8°C, then cool the material to 0°C, freeze the suspension...
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