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Powder surface cleaning equipment and cleaning method

A surface cleaning and powder technology, applied in the field of materials, can solve the problems of large powder loss, reduced filtration rate, complicated operation, etc., and achieve the effects of reducing anions and cations, high cleaning efficiency, and simple operation

Active Publication Date: 2011-04-06
WENZHOU HONGFENG ELECTRICAL ALLOY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

People have used different methods to prepare various nano-powders, but after the powder synthesis reaction is completed, a variety of anions and cations remain in the solution, and if they are not cleaned, the performance of the nano-powders will be affected
[0003] After searching the existing technology, Dong Qiang and Ji Zhaoquan published an article in the Supplement of "Journal of Silicates" on October 30, 2002 - "Basic Research on the Cleaning Process of Nano-ceramic Powder Prepared by Wet Chemical Method". It is proposed that due to the small particle size, large specific surface area, and strong surface physical and chemical effects of powder particles, there is a strong tendency to agglomerate. The traditional separation method using filter cloth as the filter medium should be used for residual ion cleaning, such as plate and frame filter press, When performing solid-liquid separation such as centrifugation, a dense filter cake layer that blocks the filter medium will be formed, and impurity ions will be wrapped in it, making it difficult to achieve the cleaning effect. At the same time, the filtration rate will decrease rapidly, and the solid-liquid separation efficiency will be low. Large body loss

Method used

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  • Powder surface cleaning equipment and cleaning method
  • Powder surface cleaning equipment and cleaning method
  • Powder surface cleaning equipment and cleaning method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] to deal with attached Na 2 CO 3 submicron Al 2 o 3 powder (average particle size 1μm) as an example

[0030] Will Al 2 o 3The powder is placed in a circulating water pool with a filter mesh of 300 mesh, and the ultrapure water is introduced into the container space outside the tubular filter of the circulating cleaning equipment, so that the powder is placed in flowing water, and the conductivity of the water used is 10μs / cm. Then apply a voltage of 200 volts on both sides of the container to form an electric field on both sides of the container. Let the powder circulate through the electric field with the water flow, put down the metal sleeve after 5 minutes and place it between the filter screen and the electrode, and connect it with the sealing ring, then stop the water pump and cancel the electric field, and discharge the water flow between the electrode and the metal sleeve Walk. Open the water inlet valve, then introduce ultrapure water into the container s...

Embodiment 2

[0032] Take the treatment of nano-TiC powder (average particle size 10nm) attached with NaCl as an example

[0033] Put the TiC powder in the circulating water pool, the filter mesh is 600 mesh, introduce the ultrapure water into the container space outside the tubular filter of the circulating cleaning equipment, put the powder in the flowing water, and the conductivity of the water used is 15μs / cm. Then apply a voltage of 400 volts on both sides of the container to form an electric field on both sides of the container. Let the powder circulate through the electric field with the water flow, put down the metal sleeve after 10 minutes, place it between the filter screen and the electrode, and connect it with the sealing ring, then stop the water pump and cancel the electric field, and discharge the water flow between the electrode and the metal sleeve Walk. Open the water inlet valve, then introduce ultrapure water into the container space outside the tubular filter, and cl...

Embodiment 3

[0035] Take the treatment of diamond powder with KCl attached (average particle size is 100μm) as an example

[0036] Put the diamond powder in the circulating water pool, the filter mesh is 50 mesh, introduce the ultrapure water into the container space outside the tubular filter of the circulating cleaning equipment, put the powder in the flowing water, and the conductivity of the used water flow is 10μs / cm. Then apply a voltage of 400 volts on both sides of the container to form an electric field on both sides of the container. Let the powder circulate through the electric field with the water flow, put down the metal sleeve every 10s and place it between the filter screen and the electrode, and connect it with the sealing ring, then stop the water pump and cancel the electric field, and the water flow between the electrode and the metal sleeve row away. Open the water inlet valve, then introduce ultrapure water into the container space outside the tubular filter, and clo...

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Abstract

The invention discloses powder surface cleaning equipment and cleaning method in the technical field of materials. The equipment comprises a circulating water inlet, a metal sleeve, a water inlet valve, an electric field anode, a filter screen, a water outlet valve, a circulating water outlet, a circulating pool, a stirring blade, a water pump, a circulating water outlet valve, a reclaiming valve, a reclaiming pipeline, a sealing ring, an electric field cathode, a circulating water inlet valve and an electric field separation container. The method, based on an ionic electric migration technology, realizes the separation of zwitterions and achieves the aim of removing ions from the powder surface. In the realization process, under the action of an electric field, the zwitterions leave awayfrom the surface of powder particles and go close to both ends of an electrode so as to separate the zwitterions from the powder. The suitable powder has the granularity of 10nm-100 microns and adopts non-conductive or conductive powder. Compared with the traditional method which singly relays on filtration and a plurality of repeated flushing in clear water, the invention has the advantages of high cleaning efficiency, good cleaning effect, convenient operation and simple equipment.

Description

technical field [0001] The invention relates to equipment and methods in the field of material technology, in particular to a powder surface cleaning equipment and cleaning method. Background technique [0002] With the continuous development of material technology, the application of submicron and even nanometer powders is becoming more and more extensive. Due to the huge specific surface area of ​​submicron or nanometer powder, the surface effect and interface effect show many unique physical and chemical characteristics, and can be made into various shapes such as spherical, polygonal, and thin slices according to the application. Such powders Materials have been widely used in chemical catalysis, electromagnetism, optics, mechanics, electronic information, fuel cells and biomedicine. People have used different methods to prepare various nano-powders, but after the powder synthesis reaction is completed, a variety of anions and cations remain in the solution, and if they...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B08B7/00
Inventor 陈乐生甘可可祁更新陈晓
Owner WENZHOU HONGFENG ELECTRICAL ALLOY
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