Thermal expansion type removable acrylic pressure-sensitive adhesive tape or sheet and method of removal
A re-peelable, heated foaming technology, applied in the direction of adhesive heating, bonding method, adhesive type, chemical instrument and method, etc. power and other issues
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preparation example 1
[0251] 90 parts by weight of 2-ethylhexyl acrylate, 10 parts by weight of acrylic acid, 0.05 parts by weight of a photoinitiator (trade name "Irgacure 184", manufactured by Ciba Specialty Chemicals), photoinitiator (trade name "Irgacure 651" , manufactured by Ciba Specialty Chemicals Co., Ltd.) 0.05 parts by weight were added into a four-necked flask, and exposed to ultraviolet rays under a nitrogen atmosphere to carry out photopolymerization, thereby obtaining a partially polymerized monomer slurry with a polymerization degree of 7%.
[0252] To 100 parts by weight of the partially polymerized monomer slurry, 30 parts by weight of a thermal foaming agent (heat-expandable microspheres, trade name "Mazumochi Microsufea F-50D", manufactured by Matsumoto Yushi Pharmaceutical Co., Ltd.), trimethylol 0.5 part by weight of propane triacrylate was uniformly mixed to obtain a heat blowing agent-containing adhesive composition (sometimes referred to as "heat blowing agent-containing adh...
preparation example 2
[0254] 90 parts by weight of 2-ethylhexyl acrylate, 10 parts by weight of acrylic acid, 0.05 parts by weight of a photoinitiator (trade name "Irgacure 184", manufactured by Ciba Specialty Chemicals), photoinitiator (trade name "Irgacure 651" , manufactured by Ciba Specialty Chemicals Co., Ltd.) 0.05 parts by weight were added into a four-necked flask, and exposed to ultraviolet rays under a nitrogen atmosphere to carry out photopolymerization, thereby obtaining a partially polymerized monomer slurry with a polymerization degree of 7%.
[0255] To 100 parts by weight of the partially polymerized monomer slurry, 30 parts by weight of a thermal foaming agent (heat-expandable microspheres, trade name "Mazumochi Microsufea F-50D", manufactured by Matsumoto Yushi Pharmaceutical Co., Ltd.), trimethylol 0.2 parts by weight of propane triacrylate was uniformly mixed to obtain a thermal foaming agent-containing adhesive composition (sometimes referred to as "thermal foaming agent-contain...
Embodiment 1
[0273] The thermal foaming agent adhesive composition (A) is applied to the release treatment surface of the process separator (B) so that the thickness after curing is 100 μm, and the thermal foaming agent composition (A) is obtained on the process separator (B). Foaming Agent Adhesive Composition Layer Ply with Thermal Foaming Agent Adhesive Composition.
[0274] The bubble-containing particle-containing polymerizable composition (A) is coated on the release treatment surface of the process separator (A) so that the thickness after curing is 800 μm, and the particle-containing polymer composition having mixed bubbles is obtained on the process separator (A). The mixed bubbles of the polymeric composition layer contain particles of the polymeric composition layer.
[0275] On one side of the peelable film (A), stick the layer sheet of the polymerizable composition containing bubbles in the form of contacting the layer of the polymerizable composition containing bubbles mixed ...
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Abstract
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