Detection method of Santanning syrup

A detection method and syrup technology, which is applied in the field of quality detection of Santanning syrup, can solve the problems of no quality index, high price, and decline in drug efficacy, and achieve safe and effective drug use

Inactive Publication Date: 2010-12-01
SICHUAN FENGCHUN PHARMA
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  • Abstract
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Problems solved by technology

However, the original standard did not carry out any quality control on the chemical medicines and traditional Chinese medicines in the prescription, neither the quality indicators nor the identification and detection methods of these quality indicators
Unscrupulous manufacturers do not strictly follow the dosage of prescriptions when producing medicines; they wantonly reduce high-priced raw materials, especially now that ephedrine hydrochloride is a chemical raw material that is strictly controlled by the state, and the price is also high. Unscrupulous manufacturers may invest less or not. Ephedrine hydrochloride causes a significant decline in the efficacy of the drug, affects the safety and effectiveness of the drug, and seriously damages the interests of patients

Method used

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  • Detection method of Santanning syrup
  • Detection method of Santanning syrup
  • Detection method of Santanning syrup

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Experimental program
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Effect test

Embodiment Construction

[0156] [Prescription] Bellflower 50g; Polygala (manufactured) 10g; Morus alba 16g; Ammonium chloride 10g; Ephedrine hydrochloride 0.5g; Menthol 0.1g.

[0157] [Preparation method] The above six flavors, Cortex Mori, Platycodon grandiflorum and Polygala were crushed into coarse powder, soaked with 375ml of 35% ethanol for 48 hours, collected the soaking liquid, stood still, and filtered. Take 650g of sucrose, add water to boil, filter, add ammonium chloride, ephedrine hydrochloride, sodium benzoate 3g, appropriate amount of caramel, stir well, filter while it is hot, let it cool, add impregnating liquid and mulberry essence ethanol solution (the amount of mulberry essence , chloroform 3.4g, menthol, ethanol 16.5ml make), stir well, add water to make 1000ml, stir well, to obtain final product.

[0158] 【Properties】This product is a light brown viscous liquid; the gas is fragrant and the taste is sweet.

[0159] 【identification】

[0160] (1) Take 2ml of this product, add 10ml o...

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Abstract

The invention provides a detection method of Santanning syrup, which comprises the steps of the physicochemical distinguishing of ammonium chloride, thin layer distinguishing of the root bark of white mulberry, the thin layer distinguishing of the menthol crystal, the content determination of ephedrine hydrochloride and the content determination of ammonium chloride. The invention effectively controls the quality of the main components such as the root bark of white mulberry, the ammonium chloride, the ephedrine hydrochloride and the menthol crystal in the prescription, not only can better and more comprehensively reflect the quality of the Santanning syrup, but also can effectively prevent the illegal manufacturer from producing the adulterant Santanning syrup, thereby ensuring the pharmacy safety of the masses.

Description

Technical field: [0001] The invention relates to a quality detection method for Santanning syrup, which belongs to the technical field of quality control of medicines. Background technique: [0002] Santanning syrup is a variety recorded in the seventh volume of traditional Chinese medicine preparations in the "Drug Standards of the Ministry of Health". The standard number is WS3-B-1439-93. , ephedrine hydrochloride, and menthol are compound syrups of Chinese and Western medicines. It has the effects of clearing the lung, relieving cough and relieving asthma. It is clinically used for the treatment of respiratory diseases such as bronchitis and cough with excessive phlegm. However, the original standard did not carry out any quality control on the chemical medicines and traditional Chinese medicines in the prescription, neither the quality indicators nor the identification and detection methods of these quality indicators. Unscrupulous manufacturers do not strictly follow...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K36/69G01N30/90G01N30/36G01N21/82G01N21/78A61P11/00A61P11/14A61P11/10A61P11/06A61K31/045A61K31/137A61K33/02
Inventor 黎勇钟茂团温国梁邹波古莉唐终国林剑
Owner SICHUAN FENGCHUN PHARMA
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