Preparation method of PS-TiO2-ATP organic/inorganic composite film
An inorganic composite, ps-tio2-atp technology, applied in the field of organic/inorganic composite film material, PS-TiO2-ATP organic/inorganic composite film preparation, can solve problems such as difficulty in uniform dispersion of particles, easy agglomeration of nanoparticles, etc. Achieve the effect of overcoming easy agglomeration, overcoming agglomeration behavior, and being easy to popularize and apply
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Embodiment 1
[0030] Preparation of PS-TiO by Ultrasonic Mixed Evaporation 2 -ATP organic / inorganic composite film, which is used in solar thin film batteries and other fields.
[0031] In this example, PS, TiO 2 and ATP as the main raw material, with C 6 h 12 As a solvent, the specific preparation steps are as follows:
[0032] (1) Obtain ATP and TiO by co-precipitation method 2 TiO with a mass ratio of 15:85 2 / ATP composite powder, in which TiO 2 The particle size is 20nm; Among them, the co-precipitation method prepares TiO 2 The specific steps of / ATP composite powder are as follows: firstly, the attapulgite clay mineral is processed, crushed, sieved, and suspended to obtain the attapulgite clay powder; secondly, the TiO2 is prepared by hydrolysis 2 Sol; then, the attapulgite clay powder ATP and TiO 2 The sol is compounded to obtain TiO 2 / ATP composite precursor, ATP and TiO 2 The mass ratio is 15:85; finally, TiO 2 / ATP composite precursor obtained TiO by high temperature ...
Embodiment 2
[0038] Preparation of PS-TiO by Ultrasonic Mixed Evaporation 2 -ATP organic / inorganic composite thin film, which can be used in thermoelectric conversion and other fields.
[0039] In this example, PS, TiO 2 and ATP as the main raw material, with C 6 h 12 As a solvent, the specific preparation steps are as follows:
[0040] (1) Obtain ATP and TiO by co-precipitation method 2 TiO with a mass ratio of 10:90 2 / ATP composite powder, in which TiO 2 The particle size is 60nm; among them, the co-precipitation method prepares TiO 2 The specific steps of / ATP composite powder are as follows: firstly, the attapulgite clay mineral is processed, crushed, sieved, and suspended to obtain the attapulgite clay powder; secondly, the TiO2 is prepared by hydrolysis 2 Sol; then, the attapulgite clay powder ATP and TiO 2 The sol is compounded to obtain TiO 2 / ATP composite precursor, ATP and TiO 2 The mass ratio is 10:90; finally, TiO 2 / ATP composite precursor obtained TiO by high tem...
Embodiment 3
[0046] Preparation of PS-TiO by Ultrasonic Mixed Evaporation 2 -ATP organic / inorganic composite film, which can be used in electromagnetic shielding, microwave absorption and other fields.
[0047] In this example, PS, TiO 2 and ATP as the main raw material, with C 6 h 12 As a solvent, the specific preparation steps are as follows:
[0048] (1) Obtain ATP and TiO by co-precipitation method 2 TiO with a mass ratio of 5:95 2 / ATP composite powder, in which TiO 2 The particle size is 100nm; Among them, the co-precipitation method prepares TiO 2 The specific steps of / ATP composite powder are as follows: firstly, the attapulgite clay mineral is processed, crushed, sieved, and suspended to obtain the attapulgite clay powder; secondly, the TiO2 is prepared by hydrolysis 2 Sol; then, the attapulgite clay powder ATP and TiO 2 The sol is compounded to obtain TiO 2 / ATP composite precursor, ATP and TiO 2 The mass ratio is 5:95; finally, TiO 2 / ATP composite precursor obtained...
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Abstract
Description
Claims
Application Information
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