Preparation method of PS-TiO2-ATP organic/inorganic composite film

An inorganic composite, ps-tio2-atp technology, applied in the field of organic/inorganic composite film material, PS-TiO2-ATP organic/inorganic composite film preparation, can solve problems such as difficulty in uniform dispersion of particles, easy agglomeration of nanoparticles, etc. Achieve the effect of overcoming easy agglomeration, overcoming agglomeration behavior, and being easy to popularize and apply

Inactive Publication Date: 2012-01-25
HUAIYIN INSTITUTE OF TECHNOLOGY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The disadvantage is that because the nanoparticles are easy to agglomerate, it is difficult to achieve uniform dispersion of the particles during blending

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] Preparation of PS-TiO by Ultrasonic Mixed Evaporation 2 -ATP organic / inorganic composite film, which is used in solar thin film batteries and other fields.

[0031] In this example, PS, TiO 2 and ATP as the main raw material, with C 6 h 12 As a solvent, the specific preparation steps are as follows:

[0032] (1) Obtain ATP and TiO by co-precipitation method 2 TiO with a mass ratio of 15:85 2 / ATP composite powder, in which TiO 2 The particle size is 20nm; Among them, the co-precipitation method prepares TiO 2 The specific steps of / ATP composite powder are as follows: firstly, the attapulgite clay mineral is processed, crushed, sieved, and suspended to obtain the attapulgite clay powder; secondly, the TiO2 is prepared by hydrolysis 2 Sol; then, the attapulgite clay powder ATP and TiO 2 The sol is compounded to obtain TiO 2 / ATP composite precursor, ATP and TiO 2 The mass ratio is 15:85; finally, TiO 2 / ATP composite precursor obtained TiO by high temperature ...

Embodiment 2

[0038] Preparation of PS-TiO by Ultrasonic Mixed Evaporation 2 -ATP organic / inorganic composite thin film, which can be used in thermoelectric conversion and other fields.

[0039] In this example, PS, TiO 2 and ATP as the main raw material, with C 6 h 12 As a solvent, the specific preparation steps are as follows:

[0040] (1) Obtain ATP and TiO by co-precipitation method 2 TiO with a mass ratio of 10:90 2 / ATP composite powder, in which TiO 2 The particle size is 60nm; among them, the co-precipitation method prepares TiO 2 The specific steps of / ATP composite powder are as follows: firstly, the attapulgite clay mineral is processed, crushed, sieved, and suspended to obtain the attapulgite clay powder; secondly, the TiO2 is prepared by hydrolysis 2 Sol; then, the attapulgite clay powder ATP and TiO 2 The sol is compounded to obtain TiO 2 / ATP composite precursor, ATP and TiO 2 The mass ratio is 10:90; finally, TiO 2 / ATP composite precursor obtained TiO by high tem...

Embodiment 3

[0046] Preparation of PS-TiO by Ultrasonic Mixed Evaporation 2 -ATP organic / inorganic composite film, which can be used in electromagnetic shielding, microwave absorption and other fields.

[0047] In this example, PS, TiO 2 and ATP as the main raw material, with C 6 h 12 As a solvent, the specific preparation steps are as follows:

[0048] (1) Obtain ATP and TiO by co-precipitation method 2 TiO with a mass ratio of 5:95 2 / ATP composite powder, in which TiO 2 The particle size is 100nm; Among them, the co-precipitation method prepares TiO 2 The specific steps of / ATP composite powder are as follows: firstly, the attapulgite clay mineral is processed, crushed, sieved, and suspended to obtain the attapulgite clay powder; secondly, the TiO2 is prepared by hydrolysis 2 Sol; then, the attapulgite clay powder ATP and TiO 2 The sol is compounded to obtain TiO 2 / ATP composite precursor, ATP and TiO 2 The mass ratio is 5:95; finally, TiO 2 / ATP composite precursor obtained...

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Abstract

The invention discloses a preparation method of a PS-TiO2-ATP organic / inorganic composite film. Polystyrene (PS), titanium dioxide (TiO2) and attapulgite (ATP) are taken as main raw materials, and cyclohexane (C6H12) is taken as solvent. The preparation method comprises the steps of: firstly, dissolving PS in C6H12 to obtain a solution A; secondly, dispersing nanometre TiO2 / ATP composite power bodies in the C6H12 to obtain a solution B; thirdly, ultrasonically mixing the solutions A and B to obtain a solution C; fourthly, pouring the solution C on a cleaned sheet to be spin coated into the film; and finally, drying the film by airing naturally, and carrying out heat treatment at the temperature of 100 to 110 DEG C to prepare the PS-TiO2-ATP organic / inorganic composite film. The film can be applied to the fields of photocatalysis, solar energy film batteries, photoelectric conversion, thermoelectric conversion, electromagnetic shielding, microwave absorption, and the like.

Description

technical field [0001] The invention relates to a preparation method of a polymer-based functional composite material, in particular to an organic / inorganic composite film material with photoelectric, thermoelectric conversion, electromagnetic shielding, and microwave absorption, specifically PS-TiO 2 -The preparation method of ATP organic / inorganic composite thin film. Background technique [0002] Polymer-based functional composites are a research and development hotspot of polymer modification. Polymer-based composite materials with multiple functions such as photoelectricity, thermoelectric conversion, electromagnetic shielding, and microwave absorption have a wide range of applications. [0003] Nano-TiO 2 It has high photocatalytic redox ability, and has application prospects in photocatalytic degradation, solar cells, and thermoelectric fields. Attapulgite clay (ATP) is a silicate clay mineral and a natural one-dimensional nanostructure. Its main characteristics ar...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08L25/06C08K13/04C08K7/10C08K3/22C08J5/18
Inventor 丁红燕周广宏章跃林岳宾陈露露周中超
Owner HUAIYIN INSTITUTE OF TECHNOLOGY
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