Wiring board, semiconductor device, and process for producing semiconductor device
A wiring substrate and manufacturing method technology, applied in semiconductor/solid-state device manufacturing, semiconductor devices, semiconductor/solid-state device components, etc., can solve the problems of reducing the adhesion of insulating films, lowering yield and reliability, and not yet achieved, etc. Problems, to achieve the effect of improving yield and reliability, and improving adhesion
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[0119] Preparation of the first insulating film forming material
[0120] 10 g of polycarbosilane ("NIPSI-L", manufactured by Nippon Carbon Co., Ltd., weight average molecular weight = about 400), 60 g (0.6 mol) of methyl isobutyl ketone, and 9 g (0.2 mol) of ) ethanol, at a constant temperature of 60°C, using a dropping funnel and under the condition of 2ml / min, drop 60-61% by mass of 10g nitric acid aqueous solution (0.1mol in water) dripping, and carry out 7-hour aging after the dripping ends reaction.
[0121] Next, using a separatory funnel, the reactant was dissolved in diethyl ether, a large amount of water and sodium bicarbonate were added, and water was washed until the pH became 5 to remove excess nitric acid. In order to remove the water used to remove nitric acid, after filtering, 200 ml of methyl isobutyl ketone was added, and diethyl ether was removed with a rotary evaporator until the reaction solution became 100 ml, thereby preparing a first insulating film ma...
Embodiment 1
[0129]
[0130] The multilayer wiring and semiconductor device of the present invention are produced as follows. First, if Figure 2A As shown, the element isolation film 12 is formed on the semiconductor substrate 10 by the LOCOS (LOCal Oxidation of Silicon) method. Based on the element separation film 12, an element region 14 is defined. In addition, a silicon substrate is used as the semiconductor substrate 10 .
[0131] Next, on the element region 14 , a gate electrode 18 is formed through the gate insulating film 16 . Next, side wall insulating films 20 are formed on the side surfaces of the gate electrodes 18 . Furthermore, impurities are introduced into the semiconductor substrate 10 using the sidewall insulating film 20 and the gate electrode 18 as a mask, thereby forming source / drain diffusion layers 22 in the semiconductor substrate 10 on both sides of the gate electrode 18 . As a result, transistor 24 including gate 18 and source / drain diffusion layer 22 is fo...
Embodiment 2
[0163]Manufacturing of multilayer wiring and semiconductor devices, adhesion-enhancing layer and second Detection method of Si-CxHy-Si bonding in two insulating films and evaluation method of adhesion (number of film peelings and adhesion strength). The results are shown in Table 1.
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