Silicon nitride ferrovanadium and production method thereof
A technology of silicon nitride ferro-vanadium and its production method, which is applied in the field of silicon nitride ferro-vanadium alloy and its production, can solve the problems of rapid nitrogen increase and stable nitrogen absorption in steelmaking, etc., and achieve easy promotion, simple process, high density big effect
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example 1
[0022] Example 1: Take 100kg of ferrosilicon powder containing 75% silicon and 150kg of ferrosilicon powder containing 50% vanadium, mix them in a V-type mixer, and send them into a resistance furnace. The temperature control is: 800°C for 2 hours, Insulate at 1200°C for 4 hours, at 1550°C for 4 hours, nitrogen pressure 0.03Mpa. Cool under protective atmosphere to obtain ferrosilicon nitride, the composition is: V 23.21%, Si 22.45%, N 22.19%.
example 2
[0023] Example 2: Take 98% V 2 o 5Powder 230kg 80kg iron fine powder containing 61% iron, 150kg ferrosilicon powder 75, 95kg graphite powder, mix evenly, add 2% polyvinyl alcohol aqueous solution 82kg, press into Ф35mm balls, cool for 5 days, bake in a resistance furnace at 120°C Bake for 2 hours, put it into the reduction nitriding sintering resistance furnace, pass nitrogen protection, heat to 750°C and keep it for 3 hours, raise the temperature to 1300°C and keep it for 5 hours, continue to heat up to 1550°C and keep it for 4 hours, nitrogen pressure 0.04MPa, protection Cooling under the atmosphere to obtain silicon nitride iron vanadium, the composition is: V 30.46%, Si27.63% N 25.75%.
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