Poly(ethylene carbonate) type polyurethane water-based adhesive
A technology of polyethylene carbonate and water-based adhesives, applied in the direction of polyurea/polyurethane adhesives, adhesive types, adhesives, etc. problems, to achieve the effect of excellent bonding strength, high storage stability, and broad market application space
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Embodiment 1
[0017] A kind of polyethylene carbonate type polyurethane aqueous adhesive is characterized in that, it is made by following method:
[0018] Take 100 parts by weight of dehydrated polyethylene carbonate diol, add 2-10 parts of dimethylol propionic acid, stir under nitrogen protection and slowly heat up to 100-120 ° C, wait for dimethylol propionic acid After the acid is completely dissolved, cool down to 50-70°C, add 20-60 parts of diisocyanate dropwise, raise the temperature to 70-80°C, and react for 2-3 hours. When the glue has a certain viscosity and becomes transparent, stop heating and let it cool naturally. At 40-50°C, stop the nitrogen flow, add 100-700 parts of 5-30% triethylamine aqueous solution under vigorous stirring, neutralize and emulsify, and obtain a milky white polyethylene carbonate polyurethane water-based adhesive.
[0019] The polyethylene carbonate diol described above is formed by copolymerizing carbon dioxide with ethylene oxide under the action of an...
Embodiment 2
[0024] Take 100 parts by weight of dehydrated polyethylene carbonate diol with a molecular weight of 3000, add 3 parts of dimethylol propionic acid, stir under nitrogen protection and slowly heat up to 110 ° C, and wait for the dimethylol propionic acid After it is completely dissolved, cool down to 50°C, add 30 parts of toluene diisocyanate dropwise, heat up to 70°C, and react for 2 hours. When the glue has a certain viscosity and becomes transparent, stop heating, cool naturally to 40°C, and stop nitrogen flow. Add 200 parts of 5% triethylamine aqueous solution under vigorous stirring, neutralize and emulsify, and obtain milky white polyethylene carbonate type polyurethane water-based adhesive.
[0025] The color of the prepared adhesive is milky white, and its mechanical stability is continuous centrifugation for 15 minutes at a speed of 3000 rpm with an 8000-type centrifuge without any separation. Freeze in a -40°C refrigerator, thaw at room temperature, and repeat 3 times...
Embodiment 3
[0027] Take 100 parts of dehydrated polyethylene carbonate diol with a molecular weight of 4000, add 2 parts of dimethylol propionic acid, stir under the protection of nitrogen and slowly heat up to 120 ° C, after the dimethylol propionic acid is completely dissolved , lower the temperature to 55°C, add 70 parts of diphenylmethane diisocyanate dropwise, raise the temperature to 80°C, and react for 2.5 hours. When the glue has a certain viscosity and becomes transparent, stop heating, cool naturally to 40°C, and stop nitrogen flow. Add 200 parts of 7% triethylamine aqueous solution under vigorous stirring, neutralize and emulsify, and obtain a milky white polyethylene carbonate type polyurethane water-based adhesive.
[0028] The color of the prepared adhesive is milky white, and its mechanical stability is continuous centrifugation for 15 minutes at a speed of 3000 rpm with an 8000-type centrifuge without any separation. Freeze in a -40°C refrigerator, thaw at room temperature...
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