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A kind of method that prepares nano titanium dioxide film on the surface of polyester fabric

A technology of nano-titanium dioxide and polyester fabrics, which is applied to the surface treatment of polyester fabrics. In the field of preparing nano-titanium dioxide films on the surface of polyester fabrics, it can solve the problems of fabric hand feeling and poor washing resistance, and achieve excellent UV resistance and washing resistance. Improved performance and good results

Inactive Publication Date: 2011-12-14
XI'AN POLYTECHNIC UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The purpose of the present invention is to provide a method for preparing a nano-titanium dioxide film on the surface of polyester fabrics, which solves the problems of polyester fabrics obtained by the existing modification methods in terms of anti-ultraviolet and antibacterial performance, poor washing resistance and fabric hand style decline.

Method used

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  • A kind of method that prepares nano titanium dioxide film on the surface of polyester fabric
  • A kind of method that prepares nano titanium dioxide film on the surface of polyester fabric
  • A kind of method that prepares nano titanium dioxide film on the surface of polyester fabric

Examples

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Embodiment 1

[0032] Weigh 4.8g of polyester fabric, 4.8g of titanium sulfate and 12g of urea respectively. The polyester fabric was washed with a mixed solution of deionized water and absolute ethanol with a volume ratio of 1:1 at a temperature of 60°C for 10 minutes under ultrasonic vibration at 28KHz and a power of 100W, and dried at 80°C. Weigh the silane coupling agent KH-560 according to 0.5% of the fabric mass, dissolve it in absolute ethanol and deionized aqueous solution with a volume ratio of 1:3, add polyester fabric and stir at 60°C for 1 hour, then Place it under a 25W ultraviolet lamp for 10 minutes, pre-bake at 80°C for 10 minutes, bake at 110°C for 20 minutes, and rinse once with deionized boiling water. Dissolve titanium sulfate and urea in 50ml of deionized water respectively, add the urea solution into the titanium sulfate solution and stir vigorously, then add the polyester fabric and soak for 5 minutes; put the polyester fabric together with the solution into a 200ml hi...

Embodiment 2

[0035] Weigh 4.8g of polyester fabric, 24g of titanium sulfate and 12g of urea respectively. The polyester fabric was washed with a mixed solution of deionized water and absolute ethanol with a volume ratio of 1:1 at a temperature of 80°C for 30 minutes under ultrasonic vibration at 28KHz and a power of 100W, and dried at 80°C. Weigh the silane coupling agent KH-560 according to 1.5% of the fabric mass, dissolve it in absolute ethanol and deionized aqueous solution with a volume ratio of 1:3, add polyester fabric and stir at 60°C for 3 hours, then Place it under a 25W ultraviolet lamp for 30 minutes, pre-bake at 80°C for 10 minutes, bake at 110°C for 20 minutes, and rinse with deionized boiling water for 3 times. Dissolve titanium sulfate and urea in 100ml and 50ml of deionized water respectively, add the urea solution into the titanium sulfate solution and stir vigorously, then add the polyester fabric to soak for 30min; put the polyester fabric together with the solution int...

Embodiment 3

[0038] Weigh 4.8g of polyester fabric, 15g of titanium sulfate and 12g of urea respectively. Polyester fabrics were washed with a mixed solution of deionized water and absolute ethanol with a volume ratio of 1:1 at a temperature of 70 ° C for 20 min under ultrasonic vibration at 28 KHz and a power of 100 W, and dried at 80 ° C. Weigh the silane coupling agent KH-560 according to 1.0% of the fabric mass, dissolve it in absolute ethanol and deionized aqueous solution with a volume ratio of 1:3, add polyester fabric and stir at 60°C for 2 hours, then Place it under a 25W ultraviolet lamp for 15 minutes, pre-bake at 80°C for 10 minutes, bake at 110°C for 20 minutes, and rinse twice with deionized boiling water. Dissolve urea and titanium sulfate in 50ml and 80ml of deionized water respectively, add the urea solution into the titanium sulfate solution and stir vigorously, then add the polyester fabric to soak for 20min; put the polyester fabric together with the solution into a hig...

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Abstract

The invention discloses a method for preparing a nano titanium dioxide thin film on the surface of a dacron. The method provided by the invention comprises the following steps of: firstly, ultrasonically vibrating and washing the dacron to be treated for 10-30 min at a temperature in a range of 60-90 DEG C by utilizing treating fluid under the conditions that the frequency is 28 kHz and the poweris 100 w; then drying the dacron for future use; secondly, utilizing titanium sulfate solution and urea solution to subject the dacron to a hydro-thermal reaction; finally, washing the dacron by utilizing the washing solution in the bath ratio of 1 to 30-50 for 15-30 min at a temperature of 100 DEG C; repeatedly washing the dacron by hot water and cold water and then drying to prepare the nano titanium dioxide thin film on the surface of the dacron. The method for preparing the nano titanium dioxide thin film on the surface of the dacron provided by the invention saves raw materials, is convenient for operating and has a good use effect; and the washing resistance of the modified dacron is obviously improved.

Description

technical field [0001] The invention belongs to the technical field of functional textile materials, and relates to a surface treatment method for polyester fabrics, in particular to a method for preparing a nanometer titanium dioxide film on the surface of polyester fabrics. Background technique [0002] Among many semiconductor functional inorganic materials, nano-titanium dioxide powder has broad application prospects in the fields of photocatalysis, dyes, industrial catalysis, lithium-ion secondary battery materials and photosensitive batteries due to its good photocatalytic activity and electrical properties. It has become the focus and hotspot of current nanotechnology research. The more prominent problem of nano-titanium dioxide powder materials is that they are easy to agglomerate, which leads to a decrease in photocatalytic activity and has a great impact on other properties. Therefore, the synthesis of monodisperse high-quality nano-TiO2 powder is the focus of res...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M11/46D06M13/50D06M10/08D06M101/32
Inventor 张辉朱红
Owner XI'AN POLYTECHNIC UNIVERSITY
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