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Real-time online optical measurement device and measurement method for metal elements in water body

A metal element, optical measurement technology, used in electrical excitation analysis, material excitation analysis, etc., can solve problems such as insufficient stability and selectivity, interference, and easy measurement results, achieving simple structure, reduced equipment cost, and convenient operation. Effect

Active Publication Date: 2011-12-21
CHONGQING UNIV OF POSTS & TELECOMM
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  • Abstract
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  • Application Information

AI Technical Summary

Problems solved by technology

This method only needs a simple working electrode, reference electrode, electrolytic cell and recording device. It has a fast detection speed and is suitable for on-site or on-line analysis. However, its measurement results are easily interfered by components such as organic matter in water. There are still deficiencies in terms of sex, etc.

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  • Real-time online optical measurement device and measurement method for metal elements in water body
  • Real-time online optical measurement device and measurement method for metal elements in water body
  • Real-time online optical measurement device and measurement method for metal elements in water body

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Embodiment Construction

[0011] The overall structure schematic diagram of the present invention is as figure 1 shown. A real-time on-line optical measurement device for metal elements in a water body, including a sample excitation device and an information receiving and displaying device. The sample excitation device is composed of a liquid to be tested 1, a sample pump 2, a glass tube 3, a metal rod 4, and a high-voltage power supply 5. The liquid to be tested constitutes a discharge cathode, and the ablation-resistant metal rod constitutes a discharge anode. The information receiving and displaying device includes a converging lens 7 , an optical filter 8 , a photodetector 9 , a data acquisition card 10 and a computer 11 .

[0012] Driven by the sampling pump, the liquid sample to be tested enters a vertically placed capillary glass tube at a flow rate of 0.5-10ml / min. The inner diameter of the capillary glass tube can range from several hundred microns to several millimeters. The metal rod used ...

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Abstract

The invention discloses a water body metallic element real-time online detecting device. In the invention, high voltage is utilized to realize gas breakdown between a water sample to be detected and a metal anode, atmosphere pressure plasma is produced, metallic elements in the water sample enters into the plasma and are excitated to a high energy level under the action of high energy particles of the plasma and emit respective characteristic atomic spectrums in a process of transiting to a ground state from the high energy level, and selection of the metallic element characteristic atomic spectrums is realized by converting transmission wavelength of a narrow band pass filter. The types of the metallic elements in the water body are determined by analyzing wavelengths of spectrum lines, and information of element concentration can be obtained by analyzing intensity of the spectrum lines. In the invention, real-time online discriminant analysis on multiple metallic elements in the water body sample can be realized by adopting only one device, thus a detection analysis program is greatly shortened and detection efficiency and measuring accuracy are improved; and the water body metallic element real-time online detecting device disclosed by the invention is applicable to metallic ion detection of drinking water source, an industrial drain outlet and the like.

Description

technical field [0001] The invention relates to the detection and analysis of the water environment, in particular to a real-time on-line optical measurement device for metal elements in the water body. Background technique [0002] Water is an important basis for all life in nature and one of the essential substances for human survival and development. However, due to human activities and the development of industry and agriculture, various water pollution problems have received more and more widespread attention, and metal residues in water, especially heavy metal pollution, have become increasingly serious. Heavy metals such as mercury, chromium, cadmium, lead and other residues are gradually enriched in the water environment, and enter the body of consumers through the food chain for long-term excessive accumulation, posing a great threat to human safety. A large amount of environmental monitoring data needs to be provided during the treatment process. How to monitor an...

Claims

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Application Information

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IPC IPC(8): G01N21/67
Inventor 郑培超王金梅刘克铭代玉
Owner CHONGQING UNIV OF POSTS & TELECOMM
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