Organic / inorganic composite layered compound containing ruthenium 535 dye and preparation method thereof
A layered compound, inorganic composite technology, applied in organic dyes, chemical instruments and methods, azo dyes, etc., can solve the problems of application limitation, difficult to arrange, limited effect, etc., to improve selectivity, improve catalytic efficiency, The effect of extending the scope of application
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[0036] Embodiment one: Preparation of ruthenium 535 amide phenyl silica layered compound;
[0037] (1) Prepare p-aminophenyl silicon oxide-dodecylsulfate layered compound in advance; its preparation method is: first dissolve 2.88mmol of sodium laurylsulfate into 250ml of deionized water, then add 2.74mmol of p-aminophenyltrimethoxysilane, then slowly drop 0.5mol / L hydrochloric acid to adjust the pH value of the mixed solution to 2.07, and magnetically stir at room temperature for 12 days to carry out the sol-gel process; Washing with deionized water and ethanol, and drying in vacuum to obtain p-aminophenyl silicon oxide-dodecylsulfate layered structure compound;
[0038] In order to prove the chemical and three-dimensional structure of p-aminophenyl silica-dodecylsulfuric acid nanocomposite layered structure, a series of analytical experiments were carried out. Firstly, octaalkyl sulfate anion is used, and chloride anion carries out anion exchange reaction with p-aminopheny...
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