Method for measuring formaldehyde and acetaldehyde content in paper for cigarette at the same time
A formaldehyde and acetaldehyde technology, applied in the field of physical and chemical inspection of cigarette packaging materials, to achieve good linear correlation, good repeatability, and good peak shape.
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Embodiment 1
[0032] Determination of the content of formaldehyde and acetaldehyde in the hard box packing paper (determination method flow process is as follows figure 1 shown);
[0033] 1. Preparation of standard working solution
[0034] (1) Preparation of mixed standard stock solution: Weigh 200 mg of formaldehyde-2,4-dinitrophenylhydrazone and 200 mg of acetaldehyde-2,4-dinitrophenylhydrazone respectively, put them in the same 100mL volumetric flask, and use Acetonitrile was dissolved and the volume was adjusted to the mark to obtain a mixed standard stock solution;
[0035] (2) Preparation of standard working solution: pipette 0.5mL of mixed standard stock solution into a 50mL volumetric flask, dissolve and mix with acetonitrile and set the volume to the mark to obtain the first-level standard working solution; take the first-level standard working solution Add 20.00mL into a 50mL volumetric flask, dissolve and mix with acetonitrile and adjust the volume to the mark to obtain the se...
Embodiment 2
[0059] Determination of the content of formaldehyde and acetaldehyde in the soft box wrapping paper (determination method flow process is as follows figure 1 shown);
[0060] 1. Preparation of standard working solution: Weigh 200 mg of formaldehyde-2,4-dinitrophenylhydrazone and 100 mg of acetaldehyde-2,4-dinitrophenylhydrazone, and the rest are the same as in Example 1.
[0061] 2. Preparation of sample solution and blank solution
[0062] (1) Preparation of sample solution: Take a piece of soft box wrapping paper, accurately cut out the main packaging surface, and a sample with an area of 15.5cm × 10.0cm, then weigh it (accurate to 0.1mg), and put it in a 100mL triangular flask with a stopper Cut it into pieces with sterile scissors, add 50.0mL of 4% acetic acid solution, place it on a shaker, shake and extract for 30min. After standing still, accurately pipette 1.0mL of clear liquid into a 10mL volumetric flask, add 4mL of derivatization reagent, dilute to volume with a...
Embodiment 3
[0069] Determination of the content of formaldehyde and acetaldehyde in the wrapping paper (determination method flow process is as follows figure 1 shown);
[0070] 1. Preparation of standard working solution: weigh 200 mg of formaldehyde-2,4-dinitrophenylhydrazone and acetaldehyde-2,4-dinitrophenylhydrazone 200 mg, all the other are the same as in Example 1.
[0071] 2. Preparation of sample solution and blank solution
[0072] (1) Preparation of sample solution: Take a piece of wrapping paper, accurately cut out a sample with an area of 22.0cm×5.5cm in the central area of the front of the package, weigh it (accurate to 0.1mg), and place it in a 100mL conical flask with a stopper Cut it into pieces with sterile scissors, add 50.0mL of 4% acetic acid solution, place it on a shaker, shake and extract for 30min. After standing still, accurately pipette 1.0mL of clear liquid into a 10mL volumetric flask, add 4mL of derivatization reagent, dilute to volume with acetonitril...
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