Glass fiber soaking agent and preparation method thereof
A technology of glass fiber and sizing agent, applied in the field of glass fiber sizing agent and its preparation, can solve the problems such as affecting the weaving process, breaking the whole bundle of yarn, unable to protect the stress condition of the glass fiber, etc., so as to improve the physical and chemical properties and solve the problem of broken yarn Effect
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Embodiment 1
[0040] ⑴ Put about 1000 liters of pure water in a 2000 liter preparation tank (take 1500 liters of preparation as an example), pour 3.5% modified amylose and 1.5% modified amylopectin, and heat to 95 ℃ to make the starch Gelatinization, forming a starch slurry.
[0041] (2) Weigh 0.5% microcrystalline paraffin, 0.5% hydrogenated vegetable oil, 0.1% quaternary ammonium salt 1827, 0.1% Span 80, 0.05% sodium dodecylbenzenesulfonate, 0.2% modified Pour the non-toxic epoxy resin adhesive into the homogenizing tank, and use a high-speed homogenizer to stir at a high speed above 6000 R / M at 80 ° C to form a uniform emulsion.
[0042] (3) Add the homogenized emulsion into the gelatinized starch slurry in the preparation tank.
[0043] (4) Add 0.01% defoamer polyoxyethylene polyoxypropylene pentaerythritol ether, add pure water until the total amount of sizing agent is 1500 liters, keep the temperature of sizing agent at 60°C, and it can be used for wire drawing production.
[0044] ...
Embodiment 2
[0046] ⑴Put about 1000 liters of pure water in a 2000 liter preparation tank (take 1500 liters of preparation as an example), pour 4.5% modified amylose and 2.5% modified amylopectin, heat to 90 ℃ to make the starch Gelatinization, forming a starch slurry.
[0047] (2) Weigh 1.5% of microcrystalline paraffin, 1.5% of hydrogenated vegetable oil, 0.5% of quaternary ammonium salt 1231, 0.5% of Span 80, 0.1% of sodium dodecylbenzenesulfonate, and 1.0% of modified Pour the non-toxic epoxy resin adhesive into the homogenizing tank, and use a high-speed homogenizer to stir at a high speed above 6000 R / M at 70 ° C to form a uniform emulsion.
[0048] (3) Add the homogenized emulsion into the gelatinized starch slurry in the preparation tank.
[0049] (4) Add 0.02% defoamer polyoxyethylene polyoxypropanolamine ether, add pure water until the total amount of sizing agent is 1500 liters, keep the temperature of sizing agent at 65°C, and it can be used for wire drawing production.
[00...
Embodiment 3
[0052] ⑴Put about 1000 liters of pure water in a 2000 liter preparation tank (taking 1500 liters of preparation as an example), pour 2.5% modified amylose and 1.5% modified amylopectin, and heat to 95°C to make the starch Gelatinization, forming a starch slurry.
[0053] (2) Weigh 1.5% of microcrystalline paraffin, 1.5% of hydrogenated vegetable oil, 0.2% of quaternary ammonium salt 1827, 0.1% of Span 80, and 0.02% of SAS, pour them into a homogenizing tank, and use them at 80°C The high-speed homogenizer stirs at a high speed above 6000R / M to form a uniform emulsion.
[0054] (3) Add the homogenized emulsion into the gelatinized starch slurry in the preparation tank.
[0055] (4) Add pure water until the total amount of sizing agent is 1500 liters, keep the temperature of sizing agent at 60°C, and then it can be used for wire drawing production.
[0056]
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