Process for preparing high-activity semi-hydrated gypsum cementing material and gypsum product by aid of phosphorous gypsum
A technology of hemihydrate gypsum and cementitious materials, applied in the field of production of gypsum cementitious materials and gypsum products, can solve the problems of high production energy consumption, high investment, high production cost, etc., and achieve saving of operating costs, easy process control, and reliability increased effect
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[0025] Example 1:
[0026] A process for preparing high-activity semi-hydrated gypsum cementing material from phosphogypsum, which includes the following processes:
[0027] 1) Phosphogypsum pretreatment process: The phosphogypsum used in this example is a by-product of wet-process phosphoric acid production and is in powder form. Its adsorbed water content is 25%, calcium sulfate dihydrate content is 98%, and soluble phosphorus content is 0.86%. The soluble fluorine content is 0.21%, the organic content is 0.12%, the soluble phosphorus content of the phosphogypsum is 0.095%, the soluble fluorine content is 0.05%, the organic content is 0.01%, and the phosphogypsum slurry is dehydrated.
[0028] 2) Atmospheric pressure hydrothermal reaction process: the pretreated phosphogypsum slurry and crystal mordant are added to a 2.0mol / L calcium chloride solution and mixed to form a slurry. The phosphogypsum and calcium chloride solution are contained in the slurry. The mass ratio is 1:9~3:2...
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[0034] Example 2:
[0035] A process for preparing high-activity semi-hydrated gypsum cementing material with phosphogypsum. The preparation steps are basically the same as those in Example 1. The difference from Example 1 is that the mass percentage of phosphogypsum and calcium chloride solution is maintained at 1:1. The rotation speed of the stirring blade is 200 rpm, and the molar concentration of calcium chloride, the reaction temperature, the temperature of the washing hot water and the drying temperature of the slurry in the solution of the serial number 3 sample preparation process of Example 1 are sequentially changed, See Table 2 for the comparison of the content of the diacid medium crystal agent, the reaction time and the dry compressive strength of the product.
[0036] Table 2 Comparison of results of calcium chloride molar concentration, succinic acid content, reaction time and product dry compressive strength
[0037]
Example Embodiment
[0038] Example 3:
[0039] A process for preparing high-activity semi-hydrated gypsum cementing material from phosphogypsum. The preparation steps are basically the same as those in Example 1. The difference from Example 1 is that the mass ratio of phosphogypsum to calcium chloride solution is maintained at 1:1. The rotation speed of the stirring blade is 200 rpm, and the sequence number of Example 1 is changed sequentially. 3 Sample preparation process 1) The type and preparation process of the modifier in 2) The type and dosage of the crystal mordant, and the impurity content of phosphogypsum after pretreatment , The comparison of the results of the dry compressive strength of the crystal medium and the product is shown in Table 3.
[0040] Table 3 Comparison of results of dry compressive strength of phosphogypsum impurity content, crystal mordant and product after pretreatment
[0041]
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