Preparation method for cation potato starch microcrystalline wax/alkyl ketene dimer (AKD) neutral/basic sizing agent
A potato starch, cationic technology, applied in wax addition, water repellent addition, paper and other directions, can solve the problems of high price of AKD emulsion, poor market competitiveness and high price, and improve emulsion stability and sizing performance, environmental protection The effect of improved protection and improved application effect
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[0013] Example one
[0014] A preparation method of cationic potato starch microcrystalline wax / AKD medium / alkaline sizing agent includes the following steps:
[0015] In the first step, 200 grams of water, 100 grams of potato starch and 0.5 grams of fungal alpha-amylase were added to the first reactor and reacted for 1.0 hour at 50°C to obtain degraded potato starch, water, potato starch and fungal alpha-amylase. The mass ratio is 200:100:0.5, then 7 grams of sodium hydroxide is added to the first reactor, the temperature is raised to 60 ℃, 49 grams of 3-chloro-2-hydroxypropyl trimethyl ammonium chloride is added, and then the temperature is raised to React at 90°C for 2 hours, add 5 grams of acetic acid to the temperature to 50°C, then reduce to 40°C, the mass ratio of potato starch, sodium hydroxide, 3-chloro-2-hydroxypropyltrimethylammonium chloride and acetic acid is 100 :7:49:5,
[0016] In the second step, water is added to the first reactor to adjust the solid content of th...
Example Embodiment
[0019] Example two
[0020] A preparation method of cationic potato starch microcrystalline wax / AKD medium / alkaline sizing agent includes the following steps:
[0021] In the first step, 200 grams of water, 100 grams of potato starch and 0.5 grams of fungal alpha-amylase were added to the first reactor to react for 1.2 hours at 51°C to obtain degraded potato starch, water, potato starch and fungal alpha-amylase. The mass ratio is 200:100:0.5, then 7 grams of sodium hydroxide is added to the first reactor, the temperature is raised to 62 ℃, 49 grams of 3-chloro-2-hydroxypropyl trimethyl ammonium chloride is added, and then the temperature is raised to React at 91°C for 1.8 hours. Cool down to 51°C and add 5 grams of acetic acid, then reduce to 32°C. The mass ratio of potato starch, sodium hydroxide, 3-chloro-2-hydroxypropyltrimethylammonium chloride and acetic acid is 100. :7:49:5,
[0022] In the second step, water is added to the first reactor to adjust the solid content of the sy...
Example Embodiment
[0025] Example three
[0026] A preparation method of cationic potato starch microcrystalline wax / AKD medium / alkaline sizing agent includes the following steps:
[0027] In the first step, 200 grams of water, 100 grams of potato starch and 0.5 grams of fungal alpha-amylase are added to the first reactor to react for 1.4 hours at 52°C to obtain degraded potato starch, water, potato starch and fungal alpha-amylase. The mass ratio is 200:100:0.5, then 7 grams of sodium hydroxide is added to the first reactor, the temperature is increased to 64 ℃, 49 grams of 3-chloro-2-hydroxypropyl trimethyl ammonium chloride is added, and the temperature is increased to React at 92°C for 1.6 hours. Cool down to 52°C and add 5 grams of acetic acid, then reduce to 34°C. The mass ratio of potato starch, sodium hydroxide, 3-chloro-2-hydroxypropyltrimethylammonium chloride and acetic acid is 100. :7:49:5,
[0028] In the second step, water is added to the first reactor to adjust the solid content of the ...
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