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Coating device for researching vacuum spraying characteristics

A vacuum spraying and coating device technology, applied in the direction of spray discharge device, injection device, measuring device, etc., can solve the problems that it is difficult to prepare functionally gradient thin films and laminated films, the structure of testing instruments is complicated, and it is difficult to popularize and apply. Achieve the effects of small footprint, simple structure, and low manufacturing cost

Inactive Publication Date: 2012-09-26
NORTHEASTERN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Even if some vacuum injection devices are used to study the film morphology, structure and photoelectric characteristics, the test instruments used are difficult to be popularized due to the shortcomings of complex structure and high investment cost.
In addition, with the rapid development of thin film technology, functionally graded thin films and laminated films have attracted much attention due to their composition and structural compatibility, but their preparation methods are mostly physical vapor deposition (PVD) and chemical vapor deposition ( CVD) method, these two methods are difficult to prepare ideal functionally graded thin films and laminated films due to the phenomenon of high temperature diffusion, and report on specific methods and devices for preparing functionally graded thin films and laminated films by vacuum jet deposition also rarely

Method used

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  • Coating device for researching vacuum spraying characteristics
  • Coating device for researching vacuum spraying characteristics
  • Coating device for researching vacuum spraying characteristics

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0055] Embodiment 1: spray characteristics research

[0056] The above-mentioned coating device can adjust the atomization cone angle, spraying angle and spraying temperature under different conditions such as polymer concentration, gas-liquid flow ratio (pressure ratio), nozzle diameter, vacuum spray chamber pressure and temperature, distance between atomizing nozzle and substrate, substrate temperature, etc. The atomization characteristics such as beam width, jet penetration distance, rupture length, atomization velocity, droplet number density, droplet size and distribution are studied, and the influence of each spray parameter on the film forming quality is analyzed according to the atomization characteristics. The study of spray characteristics requires only an atomizing nozzle and a beaker filled with a polymer solution of known concentration and connected to the atomizing nozzle through a liquid chromatography pump. First, after completing step (1), replace the correspo...

Embodiment 2

[0058] Embodiment 2: Preparation of polymer functionally gradient film

[0059] The preparation of functionally graded films requires only one atomizing nozzle and two beakers filled with different polymer solutions. After completing the above steps (1) and (2), first, adjust the electropermanent magnet on the outer guide rail of the spray chamber fixing frame to the set position, and the distance between the atomizing nozzle and the substrate holder can be determined by the position indicated by the scale; Secondly, carry out test spraying according to step (3). In the case of ensuring the spraying effect, program the HPLC liquid chromatography pump according to the experimental requirements, mix the two polymer solutions according to a certain concentration ratio, and transport them to Atomizing nozzle; then, turn on the controller of the heating device to make the infrared heating tube and the silicone rubber heater work, the temperature of the substrate is transmitted to t...

Embodiment 3

[0060] Embodiment 3: preparation of polymer laminated film

[0061] The preparation of the polymer laminated film requires two atomizing nozzles and two beakers, and the two beakers are filled with different polymer solutions, which are respectively fed into different HPLC liquid chromatography pumps. After completing the above steps (1) and (2), firstly, adjust the electropermanent magnet to the set position, and the distance between the atomizing nozzle and the substrate is determined by the position indicated by the scale; secondly, perform test spraying according to step (3) , in the case of maintaining the spraying effect, program the HPLC liquid chromatography pump as required to realize spraying of different polymer solutions from different atomizing nozzles in different time periods; then, turn on and adjust the controller of the heating device to make the injection process The temperature and the temperature of the substrate reach the experimental set value; finally, ...

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Abstract

The invention relates to a coating device for researching vacuum spraying characteristics. The front end of a vacuum spraying chamber composed of a quartz glass tube is connected with a vacuum door provided with a compound vacuum gauge and various lead flanges, and the rear end of the vacuum spraying chamber is connected with an air extraction device by virtue of an air release valve CF (conflat) flange; two atomizing nozzles adopt two-fluid-induction-charging pneumatic-type nozzles, and a nozzle flapper provided with a lifting device is arranged in front of each atomizing nozzle; a fluid delivery device and a high-pressure nitrogen delivery device which are composed of four beakers and two HPLC (high performance liquid chromatography) pumps are arranged in two paths to be respectively connected with each atomizing nozzles; an external electromagnet is used for controlling the operations of moving, taking out and putting in a substrate in the spraying chamber; an infrared heating tube and a silicon rubber heater are used for heating; and a testing device is composed of a transmitting light source, a CCD (charge coupled discharge) high-speed camera, a PC (personal computer) machine and a temperature detection device. The coating device disclosed by the invention has a simple structure, is easy to operate, good in intuitiveness and low in cost, and can be used for performing tests and comprehensive research on the various characteristics of vacuum spraying and also for preparing a multi-substrate polymer function gradient film and laminated film in different concentration ratios.

Description

technical field [0001] The invention relates to a vacuum atomization injection device, in particular to a coating device used for the research of vacuum spray characteristics. Background technique [0002] Nano-films, especially polymer-organic nanocomposite films, as a new type of polymer material film, are widely used in the fields of polymer solar cells, electroluminescent devices, thin-film transistors and other optoelectronic devices due to their light weight, good flexibility and easy processing. Has a wide range of applications. Traditional coating processes such as evaporation and sputtering are difficult to prepare high-molecular polymer organic thin films due to problems such as high-temperature thermal ablation and chemical decomposition. Many nanotechnological processes are associated with liquid phase materials as interdisciplinary technical fields are increasingly cooperating. Solution-based thin film preparation methods mainly include spin coating method, in...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01M99/00B05B5/03B05B5/16B05B15/00
Inventor 李建昌李宏宇刘必林宫兴黎勋梁启煜
Owner NORTHEASTERN UNIV
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