Freshwater domain corresponding type anti-fouling paint composition and coating and antifouling method thereof
A technology of antifouling coatings and compositions, applied in the direction of antifouling/underwater coatings, coatings, paints containing biocide, etc., can solve the problems of unsatisfactory antifouling performance and achieve good antifouling performance and good strength Effect
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[0140] Hereinafter, although an Example demonstrates this invention more concretely, this invention is not limited to these Examples.
[0141] In addition, in the following examples and comparative examples, "parts" represent parts by weight unless the technical idea of the present invention is clearly violated.
manufacture example 1
[0142] Production Example 1——Preparation of Modified Fluorine-Containing Resin
[0143]
[0144]
[0145] The preparation method is: dissolve vinyl fluoride in 10Kg butanol and add it to the reaction kettle. Then add polychlorotrifluoroethylene and 3g of benzophthalein peroxide that became liquid after heating, stir and heat to 240°C, then slowly add raw materials other than tetrafluoroethylene, and finally add polytetrafluoroethylene and the remaining butanol , reacted at 240°C for 1h. Cool down to below 200°C and add butanone, react at 180°C until the acid value reaches 13mgKOH / g, cool down, add ionized water to dilute until the viscosity (Tu-4 cups 25°C) is 220-320s. Both feeding and reaction are operated under pressure.
[0146] The details of the raw materials of the antifouling paint composition are as follows.
[0147] Table 1
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[0149] In addition, the measurement methods of various physical properties in the following Examples etc. are as follows...
manufacture example 2
[0158] (Manufacture of metal-containing monomer A-1)
[0159] 85.4 parts of propylene glycol monomethyl ether (PGM) and 40.7 parts of zinc oxide were added to a four-necked flask equipped with a condenser, a thermometer, a dropping funnel and a stirrer, and the temperature was raised to 75° C. while stirring. Next, a mixture consisting of 50.0 parts of methyl methacrylate (MMA), 36.1 parts of acrylic acid (AA), and 5 parts of water was added dropwise from the dropping funnel at a constant speed over 3 hours. After the dropwise addition, the reaction solution turned from milky white to transparent. After further stirring for 2 hours, 36 parts of propylene glycol monomethyl ether (PGM) was added to obtain a transparent mixture solution A containing metal-containing monomer A-1.
[0160] The solid content (metal-containing monomer A-1) in the obtained mixture solution A was 44.8% by weight. The proportioning composition etc. are shown in Table 2.
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