Double-component solvent-free damping coating and its preparation method

A damping coating, solvent-free technology, applied in the field of coatings, can solve the problems of wide damping wet area, low strength of the constrained layer, good corrosion resistance, etc., and achieve the effect of easy construction and excellent corrosion resistance

Inactive Publication Date: 2013-01-16
SHANGHAI DATONG HIGH TECH MATERIALS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] my country has developed and produced damping materials since the 1960s, among which the patent number CN9110548407, the name of the invention is "a flame-retardant damping coating layer constituting a constrained damping structure, but this coating has the following disadvantages: ① The strength of the constrained layer is low, and it is often damaged at high temperatures. Cracking under the stress cycle, so as to meet the performance requirements of vibration reduction and noise reduction of the material; ②It synthesizes the constrained layer and the damping layer, and the construction process is relatively complicated. Free damping material for shock absorption and noise reduction on the vibrating surface, but its damping wet area is wide, the composite loss factor is 0.05-0.08, and the damping performance is low
Patent No. CN101955711A, the title of the invention is "a quick-drying water-based damping coating and its preparation method", which provides a preparation method for water-based damping coatings, but generally speaking, the corrosion resistance of water-based coatings on metal substrates is not as good as that of oily coatings

Method used

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  • Double-component solvent-free damping coating and its preparation method
  • Double-component solvent-free damping coating and its preparation method
  • Double-component solvent-free damping coating and its preparation method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0034] Paint material is produced in following parts by weight ratio:

[0035]

[0036] The specific steps are as follows: Stir and mix 28.0 parts of dimer acid modified epoxy resin and 28.0 parts of bisphenol A epoxy resin evenly, add 1 part of defoamer, continue to stir evenly, mix 200 mesh and 325 mesh flake mica powder according to After mixing evenly in a ratio of 1:1.5, add 26 parts to the above resin mixture, add 12.0 parts of 400 mesh calcium carbonate, 5.0 parts of graphite powder and 2.0 parts of dustproof agent in sequence, stir evenly, and grind twice with a three-roller machine. When checking that the viscosity reaches 5mm without sagging, the solvent-free damping paint can be obtained.

[0037] Produce curing agent in the following proportions:

[0038] Polyamide adduct curing agent 75.0

[0039] 400 mesh talcum powder 25.0

[0040] The specific steps are as follows: add 75.0 parts of the polyamide adduct to 25.0 parts of 400-mesh talcum powder under stirri...

Embodiment 2~4

[0043] The paint composition is as shown in Table 2:

[0044] Table 2 Embodiment 2~4 paint composition

[0045] raw material name

Example 2

Example 3

Example 4

Polyether modified epoxy resin

18.0

-

-

Rubber Modified Epoxy Resin

5.0

10.0

-

Dimer Acid Modified Epoxy Resin

-

15.0

-

Polyurethane Modified Epoxy Resin

28.0

Bisphenol A epoxy resin

30.0

25.0

23.0

Composite mica powder

26.0

22.0

26.0

calcium carbonate

16.0

18.5

16.5

graphite powder

2.0

7.0

5.0

Defoamer

1.5

1.0

1.0

Anti-dust agent

1.5

1.5

1.5

[0046] The composition ratio of curing agent is as follows

[0047]

[0048] The specific operation steps of paint material and curing agent are the same as in Example 1.

[0049] Examples 2-4 were tested, and the corresponding test ...

Embodiment 5

[0054] A method for preparing a two-component solvent-free damping coating, the method comprising the following steps:

[0055] 1) Preparation of paint

[0056] Stir and mix 15 parts by weight of ether-modified epoxy resin and 30 parts by weight of bisphenol A epoxy resin with an epoxy equivalent of 180, add a commercially available defoamer, continue to stir evenly, and then add 200 mesh and 325 30 parts by weight of composite flaky mica, 10 parts by weight of 400 mesh calcium carbonate, 2 parts by weight of graphite powder, 0.5 parts by weight of commercially available defoaming agent and commercially available dustproof agent 1 part by weight, stir evenly, grind twice with a three-roller machine, check that the viscosity reaches 5mm without sagging, and the solvent-free damping paint can be obtained;

[0057] 2) Preparation of curing agent

[0058] Add 80 parts by weight of the polyamide adduct to 30 parts by weight of talcum powder under stirring, and continue stirring f...

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PUM

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Abstract

The invention relates to a double-component solvent-free damping coating and its preparation method. The method comprises the following steps: 1, paint preparation: uniformly stirring and mixing a modified epoxy resin and a standard epoxy resin, adding an antifoaming agent, continuously uniformly stirring, sequentially adding composite sheet mica, 400 mesh calcium carbonate, graphite powder, the antifoaming agent and a dust preventive, uniformly stirring, grinding twice through using a three-roll machine, and examining the viscosity to obtain the paint of the solvent-free damping coating when the viscosity satisfies a case that no flowing appears after the scraping of 5mm of a coat; 2, curing agent preparation: adding an epoxy curing agent into talcum powder under stirring, and continuously stirring for 1-2h to obtain a uniform slurry which is the curing agent of the solvent-free damping coating; and 3, coating preparation: uniformly mixing the paint obtained in step 1 with the curing agent obtained in step 2 according to a weight ratio of the paint to the curing agent of 2:1 to obtain the solvent-free damping coating. Compared with coatings prepared through the prior art, the coating prepared in the invention has the advantages of easy construction, zero content of VOC, curing at normal temperature, high loss factor, high corrosion and vibration resistances, and the like.

Description

technical field [0001] The invention relates to a coating, in particular to a two-component solvent-free damping coating and a preparation method thereof. Background technique [0002] Damping coating is a new type of functional material capable of absorbing vibrational mechanical energy. The engines or electromechanical equipment of various mechanical equipment or transport vehicles will produce different degrees of vibration and noise when they are running, and these vibrations and noise will cause harm to the environment and personnel. Damping anti-vibration and noise reduction technology is one of the methods to effectively control vibration and noise. At the same time, these facilities operate in different environments and even in high-temperature and high-humidity environments, so these anti-noise materials must have excellent anti-corrosion effects and high-temperature resistance effects. [0003] my country has developed and produced damping materials since the 196...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09D163/02C09D163/00C09D7/12C09D5/08
Inventor 杨志英
Owner SHANGHAI DATONG HIGH TECH MATERIALS
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