Preparation method and application of magnetic composite arsenic adsorbent
An adsorbent and magnetic technology, which is applied in the field of preparation of magnetic composite arsenic adsorbent, can solve problems such as non-magnetic separation, and achieve the effects of convenient use, fast and effective arsenic removal, and thorough treatment
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[0025] Into a 500mL three-neck round bottom flask, add 200mL containing 0.10mol / L FeSO4 and 0.15mol / L FeCl 3 solution, molar ratio Fe 2+ :Fe 3+=2:3, at room temperature and under electric stirring at 240 rpm, add 2 mol / L NaOH solution dropwise to the solution until the pH reaches 10, a black precipitate is formed in the solution, continue to stir for 30 minutes, and remove the crude product with the help of a permanent magnet The magnetic nanoparticles were separated by washing with deionized water until the pH of the eluent reached 7 to obtain magnetic nanoparticles; the obtained magnetic nanoparticles were transferred back to the three-necked flask, and 200 mL of deionized water was added to ultrasonically disperse for 2 minutes, at room temperature and maintained at 300 rpm Add 0.6mol / L FeCl to the three-neck flask through two different necks at the same time at an equal flow rate of 3mL / min under electric stirring per minute. 3 +0.3mol / L MnSO 4 The mixed solution and 3m...
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