Ultra-fine grain silver alloy laminar composite and manufacturing method thereof
A technology of layered composite materials and ultra-fine grains, applied in the direction of metal layered products, chemical instruments and methods, lamination, etc., can solve problems such as short circuit, electrical noise, and accelerated material damage, so as to achieve increased service life and durability Improved abrasiveness and wide application
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Embodiment 1
[0038] Example 1: Using water atomization method to prepare AgCuNiCe alloy (the mass percentages of each component are: Cu: 8%, Ni: 0.4%, Ce: 0.15%, Ag: the balance) into AgCuNiCe alloy powder, cooling rate 1.0×10 5 C / s, the AgCuNiCe alloy powder is dried and then sieved with a screen to obtain AgCuNiCe alloy powder with an average particle size of 5μm; after 100Mpa cold isostatic pressing, the ingot is formed, and the ingot product is placed in a pure hydrogen atmosphere. After sintering at 850°C for 2 hours, extrusion is performed at a heating temperature of 600°C and an extrusion ratio of 50. After extrusion, the silver alloy is subjected to a greater amount of rolling deformation at a rolling deformation of 75% and an annealing temperature of 350°C. The next largest deformation rolling and annealing treatment, the AgCuNiCe alloy strip is made. The grain size of the AgCuNiCe alloy strip reaches 1.5μm. Then, the AgCuNiCe alloy is processed by hot-rolling composite process at 6...
Embodiment 2
[0039] Example 2: Using water atomization method to prepare AgCuNiLa alloy (the mass percentages of each component are: Cu: 1%, Ni: 0.5%, La: 0.1%, Ag: balance) into AgCuNiLa alloy powder, cooling rate 1.3×10 5 ℃ / s, the AgCuNiLa alloy powder is dried and then sieved with a screen to obtain AgCuNiLa alloy powder with an average particle size of 4.7μm; the ingot is formed by 60Mpa cold isostatic pressing, and the ingot product is placed in a pure hydrogen atmosphere. After sintering at 700°C for 2.5 hours, extrusion was performed at a heating temperature of 580°C and an extrusion ratio of 55. After extrusion, the silver alloy was subjected to a rolling deformation of 75% and an annealing temperature of 300°C. After several times of large deformation rolling and annealing treatment, AgCuNiLa alloy strip is made. The grain size of AgCuNiLa alloy strip reaches 1.4μm. Then, the AgCuNiLa alloy strip is heated at 630°C and 40% deformation The alloy strip is compounded with the copper a...
Embodiment 3
[0040] Example 3: Using water atomization method to prepare AgCuNiPr alloy (the mass percentages of each component are: Cu: 4%, Ni: 0.1%, Pr: 0.5%, Ag: balance) into AgCuNiPr alloy powder, cooling rate 1.6×10 5 ℃ / s, the AgCuNiPr alloy powder is dried and then sieved with a sieve to obtain AgCuNiPr alloy powder with an average particle size of 4.9μm; the ingot is formed by 80Mpa cold isostatic pressing, and the ingot product is placed in a pure hydrogen atmosphere. After sintering at 800°C for 3 hours, extrusion was performed at a heating temperature of 580°C and an extrusion ratio of 60. After extrusion, the silver alloy was subjected to a rolling deformation of 75% and an annealing temperature of 330°C. After several times of large deformation rolling and annealing treatment, the AgCuNiPr alloy strip is made. The grain size of the AgCuNiPr alloy strip reaches 1.4μm. Then, the AgCuNiPr is heated at 600℃ and the deformation is 35% by the hot rolling composite process. The alloy ...
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