Bismuth trioxide nanotubes prepared by microwave-assisted liquid-phase process and application thereof
A bismuth trioxide, microwave-assisted technology, applied in nanotechnology, nanotechnology, nanotechnology for materials and surface science, etc., can solve problems such as unreported tetracycline wastewater, reduce energy consumption and reaction costs, The effect of easy mass production and low synthesis temperature
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[0030] Example 1:
[0031] This example provides a microwave-assisted liquid phase method for preparing bismuth trioxide (Bi 2 O 3 ) Nanotube method, follow the steps below:
[0032] A. Weigh out 0.95g of Bi(NO 3 ) 3 ·5H 2 O and 0.45g Na 2 SO 4 , Dissolved in 40mL deionized water, ultrasonic and magnetic stirring for 1 hour to form a mixed solution;
[0033] B. Weigh 0.70 g of NaOH, add 40 mL of deionized water, and ultrasonically make it uniformly dispersed to form a transparent sodium hydroxide solution;
[0034] C. Add the transparent sodium hydroxide solution obtained in step B dropwise to the mixed solution obtained in step A under magnetic stirring;
[0035] D. Transfer the solution obtained in step C to a quartz container with a capacity of 100 mL, and place it in a microwave reactor with a microwave power of 800 W. The temperature is raised to 80° C. for 10 minutes, and the product is naturally cooled.
[0036] E. Centrifuge the product obtained in step D, and wash three times wi...
Example Embodiment
[0038] Example 2:
[0039] This example provides a microwave-assisted liquid phase method for preparing bismuth trioxide (Bi 2 O 3 ) Nanotube method, follow the steps below:
[0040] A. Weigh 1.00g of Bi(NO 3 ) 3 ·5H 2 O and 0.50g Na 2 SO 4 , Dissolved in 40mL deionized water, ultrasonic and magnetic stirring for 1 hour to form a mixed solution;
[0041] B. Weigh 0.75g of NaOH, add 40mL of deionized water, and ultrasonically make it uniformly dispersed to form a transparent sodium hydroxide solution;
[0042] C. Add the transparent sodium hydroxide solution obtained in step B dropwise to the mixed solution obtained in step A under magnetic stirring;
[0043] D. Transfer the solution obtained in step C to a quartz container with a capacity of 100 mL, and place it in a microwave reactor with a microwave power of 800 W. The temperature is raised to 100° C. for 20 min, and the product is naturally cooled.
[0044] E. Centrifuge the product obtained in step D, and wash three times with deioni...
Example Embodiment
[0046] Example 3:
[0047] This example provides a microwave-assisted liquid phase method for preparing bismuth trioxide (Bi 2 O 3 ) Nanotube method, follow the steps below:
[0048] A. Weigh out 0.95g of Bi(NO 3 ) 3 ·5H 2 O and 0.45g Na 2 SO 4 , Dissolved in 40mL deionized water, ultrasonic and magnetic stirring for 1 hour to form a mixed solution;
[0049] B. Weigh 0.75g of NaOH, add 40mL of deionized water, and ultrasonically make it uniformly dispersed to form a transparent sodium hydroxide solution;
[0050] C. Add the transparent sodium hydroxide solution obtained in step B dropwise to the mixed solution obtained in step A under magnetic stirring;
[0051] D. Transfer the solution obtained in step C to a quartz container with a capacity of 100 mL, and place it in a microwave reactor with a microwave power of 800 W. The temperature is raised to 100° C. for 20 min, and the product is naturally cooled.
[0052] E. Centrifuge the product obtained in step D, and wash three times with de...
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