Preparation method of calcium carbide slag foam glass insulation material
A technology of foam glass and thermal insulation materials, applied in glass manufacturing equipment, glass molding, manufacturing tools, etc., can solve the problems of air pollution, occupying land resources, etc., and achieve the effects of protecting the environment, making the manufacturing process simple, and reducing the cost
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example 1
[0017] Example 1, at first, uniformly mix 73% glass powder, 18% carbide slag, 3% sodium carbonate and a small amount of auxiliary additives by mass fraction, add an appropriate amount of water, and stir to obtain the batch of carbide slag foam glass; Put the above-mentioned batch materials into a heat-resistant steel mold to make a flat green body, vibrate on a vibration table for 3 minutes, put it in an oven and bake it for 4 hours, put the dried green body in a heating furnace to heat, burn The production procedure is as follows:
[0018] In the preheating stage, the temperature is raised from room temperature to 600°C at a rate of 7°C / min, and the temperature is kept for 30 minutes;
[0019] In the sintering stage, the heating rate is raised to 900°C at a rate of 12°C / min;
[0020] In the foaming stage, keep warm at a constant temperature of 900°C for 40 minutes;
[0021] Rapid cooling stage, cooling to 550°C at 15°C / min;
[0022] In the annealing stage, the cooling rate...
example 2
[0024] Example 2, at first, by mass fraction with 68% glass powder, 22% carbide slag, 4% sodium carbonate and a small amount of auxiliary additives, add an appropriate amount of water, stir to obtain the batch of carbide slag foam glass; Put the batch material into a heat-resistant steel mold to make a flat green body, vibrate on a vibration table for 4 minutes, put it in an oven and bake it for 4 hours, put the dried green body into a heating furnace for heating, and the firing procedure as follows:
[0025] In the preheating stage, the temperature is raised from room temperature to 600°C at a rate of 7°C / min, and the temperature is kept for 30 minutes;
[0026] In the sintering stage, the heating rate is raised to 850°C at a rate of 12°C / min;
[0027] In the foaming stage, keep warm at a constant temperature of 850°C for 30 minutes;
[0028] Rapid cooling stage, cooling to 600°C at 15°C / min;
[0029] In the annealing stage, the cooling rate is 1°C / min, and the temperature...
example 3
[0031] Example 3, at first, by mass fraction with 62% glass powder, 27% carbide slag, 5% sodium carbonate and a small amount of auxiliary additives, add an appropriate amount of water, stir to obtain the batch of carbide slag foam glass; Put the batch material into a heat-resistant steel mold to make a flat green body, place it on a vibration table to vibrate for 3 minutes, put it in an oven and bake it for 4 hours, put the dried green body in a heating furnace to heat, and fire The procedure is as follows:
[0032] In the preheating stage, the temperature is raised from room temperature to 600°C at a rate of 7°C / min, and the temperature is kept for 30 minutes;
[0033] In the sintering stage, the heating rate is raised to 920°C at a rate of 12°C / min;
[0034] In the foaming stage, keep warm at a constant temperature of 920°C for 20 minutes;
[0035] Rapid cooling stage, cooling to 650°C at 15°C / min;
[0036] In the annealing stage, the cooling rate is 1°C / min, and the temp...
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