Tetrapod-like zinc oxide/graphene composite material and preparation method thereof
A technology of four-needle zinc oxide and composite material, applied in the field of four-needle zinc oxide/graphene composite material and preparation thereof, can solve the problems of graphene oxide agglomeration, low efficiency of four-needle zinc oxide, etc., and avoid agglomeration , improve the effect of photocatalytic activity
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[0019] A tetrapod-shaped zinc oxide / graphene composite material is graphene nanosheets grown on the surface of tetrapod-shaped zinc oxide.
[0020] One of the preparation methods of a tetrapod-shaped zinc oxide / graphene composite material, the steps include:
[0021] Step 1: Preparation of reaction precursor
[0022] Under the protection of nitrogen, dissolve 2.97g zinc nitrate in 120ml alkaline aqueous dispersion of graphene oxide with a pH value of 8 and a concentration of 0.1mg / ml, stir until completely dissolved, add 120ml anhydrous methanol and 1.2ml poly Ethylene glycol, continue to stir for later use.
[0023] Step 2 Preparation of reaction intermediate
[0024] Put the precursor solution prepared in step 1 into a closed container, and carry out a hydrothermal reaction at 200°C. The reaction time is 6 hours. After natural cooling, it is washed with deionized water and ethanol to neutrality. After drying, zinc oxide / graphite is obtained. Ene intermediates.
[0025] Step three or ...
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