Nickel-niobium intermediate alloy and preparation method thereof
A master alloy and nickel-niobium technology, which is applied in the field of nickel-niobium master alloy and its preparation, can solve the problems of difficult separation of residues and alloy ingots, high nitrogen and oxygen content of the alloy, and low product purity, etc. Low content and good controllability
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0019] Embodiment 1: The mass percent of a kind of nickel-niobium master alloy material is as table 1: table 1
[0020]
[0021] A preparation method of a nickel-niobium master alloy material, comprising the following steps:
[0022] 1) Selection and analysis of raw materials: The raw materials are niobium pentoxide, nickel oxide, aluminum powder, sodium chlorate and the purity control of the furnace charge is shown in Table 2:
[0023] Table 2
[0024]
[0025] 2) Raw material pretreatment: Put the raw material into a drying oven and dry it at 350°C (±20°C) for 24 hours.
[0026] 3) Preparation of alumina furnace barrel: Mix alumina and binder with a certain particle size ratio evenly, knot them into shapes, and place them in a drying furnace to bake and sinter, and the baked alumina furnace barrel is cooled to 300 The temperature below ℃ is ready for use, and the storage time of the alumina furnace barrel in the air should not exceed 24 hours.
[0027] 4) Mixing: We...
Embodiment 2
[0044] The mass percent of a kind of nickel niobium master alloy material is as table 6:
[0045] Table 6
[0046]
[0047] A kind of preparation method of nickel niobium master alloy material is basically the same as embodiment 1, difference is as follows:
[0048] 1. Process conditions: Table 7
[0049] raw material baking temperature
350℃(±20℃)
raw material baking time
24 hours
Mixing time
15 minutes
Charge temperature
65℃
Reaction time
2 minutes
40 hours
150.5㎏
Broken particle size
10~30㎜
[0050] 2. Formula: Table 8
[0051] raw material
Weight (㎏)
140
74.5
Aluminum powder
70
4
Return charge
0
[0052] 3. Reaction situation: the reaction is intense, the recovery rate of niobium: 95.16%, and the recovery rate of nickel: 94.13%. ...
Embodiment 3
[0057] The mass percent of a kind of nickel-niobium master alloy material is shown in Table 10:
[0058] Table 10
[0059]
[0060] A kind of preparation method of nickel niobium master alloy material is basically the same as embodiment 1, difference is as follows:
[0061] 1. Process conditions are shown in Table 11:
[0062] Table 11
[0063] raw material baking temperature
350℃(±20℃)
raw material baking time
24 hours
Mixing time
15 minutes
Charge temperature
68℃
Reaction time
1 minute 35 seconds
40 hours
Alloy ingot weight
156.3㎏
Broken particle size
10~30㎜
[0064] 2. The formula is shown in Table 12:
[0065] Table 12
[0066] raw material
Weight (㎏)
145
70.2
Aluminum powder
73.5
3.3
Return charge
4
[0067] 3. Reaction situation: the reaction i...
PUM
| Property | Measurement | Unit |
|---|---|---|
| melting point | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
Login to View More 