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389results about How to "No segregation" patented technology

Modified aliphatic high-efficiency water-reducing agent by utilizing lignosulfonate and preparation method thereof

The invention relates to a method for preparing a modified aliphatic high-efficiency water-reducing agent by utilizing lignosulfonate, belonging to the field of concrete water-reducing agents. The invention adopts acetone and formaldehyde as condensation monomers and lignosulfonate as a modifying agent and carries out sulfonating and condensation reactions under an alkaline condition to produce anovel high-efficiency concrete water-reducing agent. The preparation method of the novel high-efficiency concrete water-reducing agent comprises the following steps: (1) adding a sulfonating agent, acetone and water to a reactor, increasing the temperature to 25-65 DEG C and reacting for 0.1-1.5 hours; (2) dipping part of formaldehyde solution for 0.25-2.5 hours, increasing the temperature to 70-95 DEG C and reacting for 1-6 hours; and (3) decreasing the temperature to below 60 DEG C, adding the lignosulfonate and the rest of the formaldehyde solution to the reactor, using an alkaline regulator to regulate a pH value of the system to be 8.0-14.0, increasing the temperature to 70-98 DEG C, reacting for 1-5 hours and decreasing the temperature before discharging. The modified aliphatic high-efficiency water-reducing agent is suitable for producing commercial concrete which has similar color as normal concrete and has smaller collapsed slump loss. By adjusting the process, such as proportioning raw materials, and the like and effectively utilizing the lignosulfonate, the invention not only decreases the product cost, but also lessens environmental pollutants and has favorable industrialized prospects.
Owner:NANJING FORESTRY UNIV

Method for producing wear-resistant composite roller

The invention relates to a method for manufacturing a wear resistant composite roll, which belongs to the technical field of steel rolling. The most difficult problems in the technology transfer of the prior combined composite roll are the improvement on the processability of an outer-layer roll sleeve and the improvement on the processing efficiency. The method comprises the following steps: opening a groove on the outer surface of a roll collar inner sleeve, washing the roll collar inner sleeve by using diluted hydrochloric acid and alcohol, then painting borax on the surface of the roll collar inner sleeve and in the groove, and air-drying the roll collar inner sleeve and placing the roll collar inner sleeve in a casting mould; pouring outer layer wear resistant molten metal through a bottom pouring method to obtain an imbedded composite roll sleeve; and combining the imbedded composite roll sleeve with a cast steel or forged steel rolling shaft through splines and integrating the imbedded composite roll sleeve and the cast steel or forged steel rolling shaft through interference fit so as to obtain the wear resistant composite roll. The composite roll has the advantages of high hardness for the outer surface layer, good wear resistance, high roll core strength, good tenacity, firm combinations between the roll sleeve and the roll core and between the roll sleeve outer surface layer and the roll collar inner sleeve and the like.
Owner:BEIJING UNIV OF TECH

Preparation method of small-particle-size uniform-aluminum-doped spherical tricobalt tetraoxide

The invention relates to a preparation method of a lithium ion battery positive electrode material precursor, in particular to a preparation method of small-particle-size uniform-aluminum-doped spherical tricobalt tetraoxide. The preparation method includes following steps: 1, adding soluble aluminum salt and EDTA disodium into a cobalt salt solution to prepare a cobalt-aluminum mixed salt complexsolution; 2, injecting pure water into a reaction kettle to serve as base liquid, blowing in air, adding a small amount of sodium hydroxide solution to adjust pH, and rising temperature; 3, adding the cobalt-aluminum mixed salt complex solution and the sodium hydroxide solution into the reaction kettle for settling reaction while stirring; 4, sampling every 2h to measure granularity till reaching2-5um after more than 40h of reaction, and filtering and washing a material after the granularity reaches a target value; 5, thermally decomposing aluminum-doped hydroxyl cobalt after being washed sectionally to finally obtain small-particle-size uniform-aluminum-doped spherical tricobalt tetraoxide with uniform distribution of aluminum from inside to outside, tricobalt tetraoxide is compact andadhesion-free spherical particles in morphology, tap density is 2.0-2.7g/cm3, and laser granularity distribution is narrow.
Owner:취저우화여우코발트뉴머터리얼컴퍼니리미티드 +1

C / C-SiC composite material and preparation method and application thereof

The present invention discloses a C / C-SiC composite material and a preparation method and application thereof. The C / C-SiC composite is a multilayer symmetrical gradient structure, the symmetrical multilayer gradient structure comprises from the inner layer to the outer layer in turn a middle layer, a longitudinally-symmetrical second layer short-cut carbon fiber reinforced silicon carbide layer and a longitudinally-symmetrical first layer short-cut carbon fiber reinforced silicon carbide layer, the carbon fiber content of the first layer short-cut carbon fiber reinforced silicon carbide layer is lower than that of the second layer short-cut carbon fiber reinforced silicon carbide layer, and the middle layer is a 90 DEG and 45 DEG plain carbon fiber cloth interlaced superposed reinforced toughened interlayer. The C / C-SiC composite is prepared from short-cut carbon fiber, plain carbon fiber cloth, phenolic resin and industrial silica fume as raw materials by compression molding, curing, carbonization and infiltration. Products prepared by the C / C-SiC composite material have high density, excellent mechanical property, oxidation resistance, friction and wear resistance and fatigue resistance, and are suitable for the fields of high end industries such as high speed and high energy transportation vehicles.
Owner:HUNAN UNIV OF TECH

Wet process for building 3t intermediate frequency electric furnace

The invention relates to a wet process for building a 3t intermediate frequency electric furnace. By the process, 3t of materials can be melted, and the service life is prolonged. The process comprises the following steps of: (1) manufacturing a steel crucible die which has a shape of a truncated hollow cone; (2) paving an insulation layer and a thermal insulation layer by using two layers of asbestos cloth; (3) paving a furnace bottom, namely paving two layers of asbestos cloth at the furnace bottom in a staggered mode; (4) paving a furnace wall, namely paving two layers of asbestos cloth next to the inner wall of an induction coil from top to bottom, ensuring that each layer is flat and does not have any wrinkle, adhering longitudinal joints for lapping by using water glass, staggering joints of two adjacent layers, and adhering the asbestos cloth which stretches out of the upper plane to a fireproof brick plane at an upper opening of the furnace by using the water glass; (5) preparing a furnace lining material from refined quartz sand; (6) manually knotting a furnace lining, brushing a layer of water glass before filling, and tamping a filler; and (7) baking the furnace and sintering, namely baking only by using firewood after the furnace is built by the wet process, adding 50 to 60kg of firewood into a hearth for several times, and completely combusting to bake the furnace lining.
Owner:HANGZHOU ZHONGQIANG ROLLER

Preparation method of molybdenum-niobium alloy sputtering target

The invention discloses a preparation method of a molybdenum-niobium alloy sputtering target. The method comprises the following steps: (1) molybdenum powder and niobium powder are put in a mixing tank of a mixing machine for uniformly mixing to obtain mixed powder; (2) the cold isostatic pressing is performed for the mixed powder to obtain a slab; and the slab is pre-sintered under the vacuum or hydrogen atmosphere protection condition to obtain a molybdenum-niobium alloy prefabricated blank; (3) the surface of the molybdenum-niobium alloy prefabricated blank is turned and milled; and the hot isostatic pressing is performed to obtain a molybdenum-niobium alloy part; and (4) the mechanical processing and the surface grinding are performed for the molybdenum-niobium alloy part to obtain the molybdenum-niobium alloy sputtering target. The preparation method is simple in process, and saves raw materials; the introduction of impurity elements can be reduced in the preparation process; the prepared molybdenum-niobium alloy sputtering target is uniform in components, free of segregation and fine in grains; the theoretic density can reach above 99%; the oxygen mass content is lower than 500 ppm; and the requirements of the sputtering target can be preferably satisfied.
Owner:JINDUICHENG MOLYBDENUM CO LTD
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