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122results about How to "Alleviate environmental pressure" patented technology

Method for producing electronic-stage hydrofluoric acid

ActiveCN101570318ASolve hard-to-remove problemsHigh purityFluorine/hydrogen-fluorideHydrofluoric acidBoiling point
The invention relates to a method for producing electronic-stage hydrofluoric acid. The method comprises the following steps: (1), preheating and roughly distilling a measured anhydrous hydrofluoric acid raw material to remove low boiling point matter; (2), using ultra-pure water to absorb hydrofluoric acid roughly distillated and exhausted from a condenser outlet to be 48 to 49 percent of hydrous hydrofluoric acid solution; (3), distilling an absorbed hydrofluoric acid semi-finished product by a fluoroplastic resin sub-boiling distiller, gasifying fluorine hydride liquid to generate ultra-pure electronic-stage hydrofluoric acid gas, condensing to be 48 to 49 percent of anhydrous hydrofluoric acid solution and remaining high boiling point matter and heavy metals at the bottom of the sub-boiling distiller; and (4), secondarily filtering the hydrofluoric acid semi-finished product output from the fluoroplastic resin sub-boiling distiller, and finally, automatically filling to prepare 48 percent of ultra-pure hydrofluoric acid finished product. The method fully utilizes the different of boiling points between the anhydrous hydrofluoric acid and various impurities in the anhydrous hydrofluoric acid to remove the impurities at different temperatures, particularly remove silicon so that the impurity content of the obtained ultra-pure hydrofluoric acid is decreased to the minimum.
Owner:DO FLUORIDE CHEM CO LTD

Ardealite road base course material and preparation method thereof

The invention discloses an ardealite road base course material and a preparation method thereof. The ardealite road base course material is prepared from the following raw materials in parts by weight: 40-80 parts of ardealite, 0.5-5 parts of diethylaminopropylamine, 0.1-0.5 part of a polycarboxylic acid water reducing agent, 10-40 parts of sandstone and 5-40 parts of water quenching slag. The preparation method comprises the following steps of: (1) dehydrating ardealite and crushing; (2) uniformly mixing the ardealite, sandstone and water quenching slag to obtain a material A; (3) uniformly mixing the polycarboxylic acid water reducing agent with the material A to obtain a material B; (4) adding the diethylaminopropylamine into the material B to obtain a material C; and (5) adding water into the material C, and stirring uniformly to obtain a finished product. In the method, the ardealite is taken as a major raw material, so that the utilization way of ardealite is expanded, the environmental protection stress is relieved, comprehensive utilization production energy consumption of ardealite is lowered, and the ardealite road base course material has a wide market prospect and is consistent with the requirements of recycling economy and sustainable development. The ardealite road base course material has the advantages of reasonable formula, simple preparation method and durability, and is suitable for road construction in ardealite-containing regions.
Owner:GUIZHOU KAILIN PHOSPHOGYPSUM INTEGRATION UTILIZATION

Process for preparing potassium borofluoride and co-production of white carbon black and sodium fluosilicate

The invention relates to a method for preparing potassium fluoborate with the co-product of white carbon black and sodium fluosilicate, which takes hydrofluosilicic acid, boric acid, industrial salt and potassium chloride as main raw materials and particularly comprises the steps as follows: (1) the hydrofluosilicic acid is firstly added into a leaching tank which is then preheated to 60 DEG C to 100 DEG C and then opened for carrying out stirring, theoretical quantity of boric acid is added into the hydrofluosilicic acid, then the leaching tank is obturated and reaction is carried out continuously for 2.0 hours to 6.0 hours, and leaching is carried out at the constant temperature of 60 DEG C to 100 DEC G; (2) qualified fluoboric acid solution after being leached is filtered, the white carbon black is dried after progressive concentration and washing by levels of water to produce the white carbon black; (3) the filtrate obtained and a first lotion are added with the industrial salt for purifying and disiliconization, then theoretical quantity of industrial salt is added for carrying out reaction for 10 minutes to 30 minutes to prepare sodium fluosilicate slurry; (4) the sodium fluosilicate slurry prepared is filtered, washed and dried to obtain sodium fluosilicate products, and the filtrate obtained is used for synthetizing the potassium fluoborate; (5) theoretical quantity of potassium chloride is added into the filtrate obtained in step (4) for carrying out reaction for 10 minutes to 30 minutes; (6) after the reaction in step (5) completes, filtration is carried out, an ointment is washed by primary water and dried to obtain the potassium fluoborate.
Owner:DO FLUORIDE CHEM CO LTD

Method for producing ultra-clean high-pure hydrofluoric acid

ActiveCN101570319ASolve hard-to-remove problemsHigh purityFluorine/hydrogen-fluorideHydrofluoric acidDistillation
The invention relates to a method for producing ultra-clean high-pure hydrofluoric acid. The method comprises the following steps: (1), emptying air in a system; (2), adding a measured liquid hydrogen fluoride raw material to a rough distillation kettle with a heat exchanger for rough distillation; (3), controlling the inside pressure of the rough distillation kettle to be lower than 0.2MPa and adding an oxidant; (4), repeatedly condensing, refluxing and vaporizing in the rough distillation kettle; (5), pumping gas guided from a top outlet of a water condenser into the bottom of a spraying absorption tower so as to be absorbed by spraying absorption liquid which is sprayed in from the top of the absorption tower; (6), gasifying and pumping hydrofluoric acid into the absorption tower to be absorbed; (7), pumping the hydrofluoric acid at the outlet of the condenser into the absorption tower and using ultra-pure water to absorb into 48 percent to 49 percent of hydrous hydrofluoric acid solution; (8), secondarily rectifying the 48 percent to 49 percent of hydrous hydrofluoric acid solution; and (9), filtering the 48 percent to 49 percent of hydrous hydrofluoric acid solution after secondary rectification at two stages to prepare 48 percent of ultra-clean high-pure hydrofluoric acid finished product. The invention not only improves the purity of the ultra-clean high-pure hydrofluoric acid, but also increases the economic benefits and the environmental-protection benefits.
Owner:DO FLUORIDE CHEM CO LTD

Method for preparing rare earth polysaccharide composite fibers

The invention provides a method for preparing rare earth polysaccharide composite fibers. The method is characterized by comprising the following specific steps: step 1, dissolving polysaccharides to prepare a spinning solution; step 2, preparing a coagulating bath, wherein the coagulating bath contains rare earth metal ions; step 3, metering the spinning solution obtained in the step 1 by virtue of a metering pump, extruding the spinning solution to enter the coagulating bath obtained in the step 2 by virtue of a spinning nozzle, wherein the polysaccharides and the rare earth metal ions are subjected to coordination complexation, and the fibers are subjected to coagulation forming; and step 4, cleaning the obtained fibers by virtue of deionized water and drying, thus obtaining the rare earth polysaccharide composite fibers. According to the method disclosed by the invention, the spinning solution with a certain concentration is prepared by utilizing the polysaccharides, the rare earth metal ions are prepared into the coagulating bath of a certain concentration, and the rare earth polysaccharide composite fibers are prepared by virtue of coordination of the polysaccharides and the rare earth metal ions. The spinneret orifice is not blocked during wet spinning, and the spinning operation has high production continuity.
Owner:DONGHUA UNIV

A kind of method for stepwise separation and high-efficiency flotation of potassium salt ore to produce KCl

ActiveCN107188200BQuality improvementEfficient quality productionAlkali metal chloridesGranularityPotassium
The invention discloses a method for efficient flotation production of KCL through sequential separation of sylvite ore, and relates to a method for producing KCl from sylvite ore. According to the technical scheme, the method comprises the steps that after the sylvite ore is manufactured into the certain granularity, pulping, desalting, coarse KCL grain separation, coarse KCl grain washing, fine KCl grain floatation, fine KCl grain washing, dehydration and drying are performed to obtain crude KCl grain products and fine KCl grain products with the purity being 95% or more are obtained; on the basis of advanced separation of some NaCl tail salt and crude KCL grains before KCL floatation or during floatation, the KCL floatation amount is decreased, the floatation strength is lowered, the equipment input is decreased, the building investment is lowered, the floatation reagent consumption is reduced, the environment-friendly pressure is relieved, the mineral separation energy consumption is reduced, the production cost is lowered, the product type is optimized, the product quality is improved, and the KCL recycling rate is increased; the method is mainly used for washing machining of carnallite and sylvine ore of deposit mining.
Owner:山东瑞源钾盐工程技术股份有限公司

Method for producing neomycin by replacing part of fermenting raw materials with soybean meal

The invention discloses a method for producing neomycin by replacing part of fermenting raw materials with soybean meal. The method consists of the following steps: (1) culturing bevel spores; (2) culturing a bevel spore suspension; (3) performing seeding tank culturing: putting the bevel spore suspension into a seed culture tank for culturing; (4) performing fermentation tank culturing: feeding a culture solution subjected to the seed tank culturing into a fermentation culture tank for culturing, wherein the culture solutions in the seed tank and the fermentation tank include soybean meal of which the mass content is 2.0-5.0 percent the mass of the culture solution in the fermentation tank, and the culture solution in the fermentation tank does not contain peptone, yeast powder and peanut powder; (5) terminating fermentation, diluting a fermentation solution, neutralizing till the pH value becomes 6.4-7.0 to obtain a diluted fermentation solution, thereby finishing the fermentation step. According to the method for producing the neomycin by replacing part of the fermenting raw materials with the soybean meal, the problems of complex raw material formula and high cost of the culture solution are solved, the formula is simplified effectively, the cost is reduced, and the production of the neomycin is guaranteed.
Owner:YICHANG SANXIA PHARMA

Manganese processing rotary kiln with gas furnace supplying heat

The invention discloses a manganese processing rotary kiln with a gas furnace supplying heat. The rotary kiln is characterized in that the rotary kiln is arranged obliquely, and is internally provided with a burner; the burner is connected with an air control valve and a gas control valve; an air-lock valve is arranged at the high end of the rotary kiln for feeding, and is connected with a dust collector through a fin section and an air pipe; the fin section is externally provided with a cover cylinder; the air pipe is externally provided with an extension-type air heat exchanger; after the cover cylinder and a lower air exhaust port of the air heat exchanger are converged, one branch is connected with the gas control valve through an air blower and the gas furnace, and the other branch is connected with the air control valve through the air blower; and the rotary kiln is internally provided with raised fire-resistant plates. The raised fire-resistant plates increase a heat transfer area of the rotary kiln, and facilitate stirring a material and reaching the reaction temperature rapidly, so that the heat efficiency is improved; the fin section and the air heat exchanger achieve waste heat utilization, and facilitate burning; rapid cooling is performed on a pellet material by a rapid cooling liquid bath, and a large amount of water can be evaporated through a reaction, so that environment protection pressure due to production liquid expansion can be alleviated effectively; and the rotary kiln is particularly suitable for burning processing of manganese ore and has broad application prospects.
Owner:JISHOU UNIVERSITY

A method of producing electronic grade hydrofluoric acid

ActiveCN101570318BSolve hard-to-remove problemsHigh purityFluorine/hydrogen-fluorideHydrofluoric acidBoiling point
The invention relates to a method for producing electronic-grade hydrofluoric acid, which specifically comprises the following steps: (1) after preheating the measured anhydrous hydrofluoric acid raw material, carry out crude distillation to remove low-boiling substances; After crude distillation, the hydrofluoric acid discharged from the outlet of the condenser is absorbed with ultrapure water, and the absorption is 48-49% aqueous hydrofluoric acid solution; Boiling distiller distillation, hydrogen fluoride liquid gasification to generate ultra-pure electronic grade hydrofluoric acid gas, condensed into 48 ~ 49% aqueous hydrofluoric acid solution, high boiling point substances and heavy metals remain at the bottom of the sub-boiling distiller; (4 ) The semi-finished product of hydrofluoric acid from the sub-boiling distiller of fluoroplastics is filtered through the second stage and finally made into 48% ultra-high-purity hydrofluoric acid finished product through automatic filling. The method of the present invention makes full use of the different boiling points of anhydrous hydrofluoric acid and impurities in anhydrous hydrofluoric acid, and removes different impurities, especially silicon, at different temperatures, so that the impurity content of the obtained ultra-high-purity hydrofluoric acid is reduced to lowest.
Owner:DO FLUORIDE CHEM CO LTD

Manganese processing rotary kiln system with gas furnace supplying heat and draught fan being free of dust accumulation

The invention discloses a manganese processing rotary kiln system with a gas furnace supplying heat and a draught fan being free of dust accumulation. A rotary kiln is arranged in an inclined mode. A combustor is arranged in the rotary kiln and connected with an air control valve and a gas control valve. An air lock is arranged at the higher end of the rotary kiln for feeding and connected with a dust remover through a fin section and an air pipe. A cover cylinder is arranged outside the fin section, a sleeve type air heat exchanger is arranged outside the air pipe, and the cover cylinder is connected with the gas control valve and the air control valve after being joined with a lower air suction port of the air heat exchanger. The draught fan is of a structure with blades being in a reverse drop shape and a back plate being in a butterfly shape. A convex refractory plate is arranged in the rotary kiln. Through the convex refractory plate, the heat transfer area of the rotary kiln is increased, material stirring is promoted, and heat efficiency is easily improved; through the fin section and the air heat exchanger, tail heat is utilized, and combustion is facilitated; through shock chilling liquid, the environmental protection pressure of production liquid expansion is effectively relieved; because the draught fan is free of dust accumulation, safety accidents are effectively eradicated. The manganese processing rotary kiln system is especially suitable for manganese ore firing processing and has broad application prospects.
Owner:JIANGSU XIYI HIGH NEW DISTRICT TECH DEV CO LTD

Method for preparing potassium fluozirconate through fluosilicic acid

The invention provides a method for preparing potassium fluozirconate through fluosilicic acid. The method comprises the steps as follows: (1) adding a fluosilicic acid solution to a leaching groove, then heating to reach 40 to 100 DEG C, starting to agitate, and adding the zirconium oxychloride with the theoretical amount to the fluosilicic acid solution; reacting and leaching for 1 to 5 hours under constant temperature condition; (2) filtering the fluosilicic acid obtained by leaching; washing the filter residue, then parching the filter residue to obtain a white carbon black product; (3) adding sodium chloride with theoretical amount to the mixture of the filtrate and the first washing water to obtain the sodium fluosilicate size; (4) filtering the obtained size, washing, and drying to obtain sodium fluosilicate; (5) adding the filtrate in step (4) into the potassium chloride solution with the theoretical amount to react for 30 to 60 minutes, and filtering to obtain paste; and (6) washing the obtained paste through water, and then parching to obtain the finished product. According to the method provided by the invention, the raw materials are easy to obtain, and low in cost, thus the producing cost can be greatly reduced; and meanwhile, the valuable white carbon black and sodium fluosilicate can be produced.
Owner:HUNAN NONFERROUS FLUORIDE CHEM

Method for efficient flotation production of KCL through sequential separation of sylvite ore

ActiveCN107188200AQuality improvementEfficient quality productionAlkali metal chloridesGranularityMachining
The invention discloses a method for efficient flotation production of KCL through sequential separation of sylvite ore, and relates to a method for producing KCl from sylvite ore. According to the technical scheme, the method comprises the steps that after the sylvite ore is manufactured into the certain granularity, pulping, desalting, coarse KCL grain separation, coarse KCl grain washing, fine KCl grain floatation, fine KCl grain washing, dehydration and drying are performed to obtain crude KCl grain products and fine KCl grain products with the purity being 95% or more are obtained; on the basis of advanced separation of some NaCl tail salt and crude KCL grains before KCL floatation or during floatation, the KCL floatation amount is decreased, the floatation strength is lowered, the equipment input is decreased, the building investment is lowered, the floatation reagent consumption is reduced, the environment-friendly pressure is relieved, the mineral separation energy consumption is reduced, the production cost is lowered, the product type is optimized, the product quality is improved, and the KCL recycling rate is increased; the method is mainly used for washing machining of carnallite and sylvine ore of deposit mining.
Owner:山东瑞源钾盐工程技术股份有限公司
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