Flax fiber degumming process

Inactive Publication Date: 2013-09-04
太仓市芸芸化纤有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the wet spinning method is mainly used in China. The process is complex, the process is long, the spinnable count is low, and the requirements for equipment are high. It is difficult to blend flax with other fibers in wet processing, and the yarn is stiff, so it is difficult to develop high-grade, For many kinds of textile products, to overcome the...

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0014] A kind of degumming process of flax fiber, comprises the following steps:

[0015] (1) High temperature and high pressure pretreatment: The flax fiber is pretreated at a temperature of 105°C and a pressure of 0.3 atmospheres, and the treatment time is 40 minutes; Less damage to fibers, resulting in low residual glue rate, high single fiber strength, effectively improving the quality of flax fibers,

[0016] (2 Washing: wash the flax fiber pretreated by high temperature and high pressure, and the treatment temperature is 40°C;

[0017] (3) Chemical degumming treatment: Sodium hydroxide solution with a mass concentration of 10g / L, hydrogen peroxide solution at 5g / L, sodium silicate solution at 5g / L, sodium carbonate solution at 5g / L and penetrant JFC-2 according to Mix the mass ratio of 2:2:2:2:1:1 to make a cooking liquid, put the washed flax fibers into the cooking liquid for degumming treatment, the cooking time is 80min, the cooking temperature is 80°C, and the liquo...

Embodiment 2

[0021] (1) High temperature and high pressure pretreatment: The flax fiber is pretreated at a temperature of 105°C and a pressure of 0.5 atmospheres, and the treatment time is 20 minutes; Less damage to fibers, resulting in low residual glue rate, high single fiber strength, effectively improving the quality of flax fibers,

[0022] (2) Washing: wash the flax fiber pretreated by high temperature and high pressure at a temperature of 50°C;

[0023] (3) Chemical degumming treatment: Sodium hydroxide solution with mass concentration of 30g / L, hydrogen peroxide solution at 10g / L, sodium silicate solution at 10g / L, sodium carbonate solution at 10g / L and penetrant JFC-2 according to Mix the mass ratio of 2:2:2:2:1:1 to make a cooking liquid, put the washed flax fiber into the cooking liquid for degumming treatment, the cooking time is 60min, the cooking temperature is 70°C, the bath ratio The ratio is 1:15; hydrogen peroxide and alkali are used to act on flax fiber, and hydrogen pe...

Embodiment 3

[0027] (1) High temperature and high pressure pretreatment: The flax fiber is pretreated at a temperature of 105°C and a pressure of 0.4 atmospheres, and the treatment time is 30 minutes; the high temperature and high pressure pretreatment method is shorter than the ordinary acid-base pretreatment method. Less damage to fibers, resulting in low residual glue rate, high single fiber strength, effectively improving the quality of flax fibers,

[0028] (2 Washing: Washing the flax fiber pretreated by high temperature and high pressure at a temperature of 45°C;

[0029] (3) Chemical degumming treatment: Sodium hydroxide solution with mass concentration of 20g / L, hydrogen peroxide solution of 8g / L, sodium silicate solution of 8g / L, sodium carbonate solution of 8g / L and penetrant JFC-2 according to Mix the mass ratio of 2:2:2:2:1:1 to make a cooking liquid, put the washed flax fiber into the cooking liquid for degumming treatment, the cooking time is 70min, the cooking temperature i...

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PUM

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Abstract

The present invention discloses a flax fiber degumming process, which adopts a process such as a high temperature and high pressure pretreatment, water washing, chemical degumming, acid washing, water washing, dehydration and drying, wherein the high temperature and high pressure pretreatment method provides characteristics of short treatment time and low damage on fibers compared to the ordinary acid alkali pretreatment method so as to provide effects of low residual gum content, high single fiber strength and effective flax fiber quality improvement, the chemical degumming process adopts hydrogen peroxide and alkali to act on flax fibers, and the hydrogen peroxide reacts with lignin to form oxidized lignin easily dissolved in an alkali liquid, such that the lignin of the fibers is effectively removed, degumming and bleaching are achieved, water and electricity resources are saved, and production efficiency is increased. With the present invention, a plurality of problems of low comprehensive long flax content, unstable quality , high residual gum content, heavy environment pollution and the like of the flax fiber finished product in the prior art are overcome, and strong application prospects are provided.

Description

technical field [0001] The invention relates to a fabric degumming process, in particular to a flax fiber degumming process. Background technique [0002] Flax fiber is the oldest textile fiber in the world, and the fabrics made of it are widely used. The fabric of flax fiber not only has excellent heat dissipation and air permeability, but also has strong hygroscopicity, so it is known as "natural air conditioner". Won the favor of consumers. At present, the wet spinning method is mainly used in China. The process is complicated, the process is long, the spinnable count is low, and the requirements for equipment are high. It is difficult to blend flax with other fibers in wet processing, and the yarn is stiff, so it is difficult to develop high-grade, For many kinds of textile products, in order to overcome the above defects, the flax fiber must be finely processed and degummed before spinning. At present, most of the traditional degumming methods such as natural water ret...

Claims

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Application Information

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IPC IPC(8): D01C1/02
Inventor 龚耀中
Owner 太仓市芸芸化纤有限公司
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