Flax fiber degumming process
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Embodiment 1
[0014] A kind of degumming process of flax fiber, comprises the following steps:
[0015] (1) High temperature and high pressure pretreatment: The flax fiber is pretreated at a temperature of 105°C and a pressure of 0.3 atmospheres, and the treatment time is 40 minutes; Less damage to fibers, resulting in low residual glue rate, high single fiber strength, effectively improving the quality of flax fibers,
[0016] (2 Washing: wash the flax fiber pretreated by high temperature and high pressure, and the treatment temperature is 40°C;
[0017] (3) Chemical degumming treatment: Sodium hydroxide solution with a mass concentration of 10g / L, hydrogen peroxide solution at 5g / L, sodium silicate solution at 5g / L, sodium carbonate solution at 5g / L and penetrant JFC-2 according to Mix the mass ratio of 2:2:2:2:1:1 to make a cooking liquid, put the washed flax fibers into the cooking liquid for degumming treatment, the cooking time is 80min, the cooking temperature is 80°C, and the liquo...
Embodiment 2
[0021] (1) High temperature and high pressure pretreatment: The flax fiber is pretreated at a temperature of 105°C and a pressure of 0.5 atmospheres, and the treatment time is 20 minutes; Less damage to fibers, resulting in low residual glue rate, high single fiber strength, effectively improving the quality of flax fibers,
[0022] (2) Washing: wash the flax fiber pretreated by high temperature and high pressure at a temperature of 50°C;
[0023] (3) Chemical degumming treatment: Sodium hydroxide solution with mass concentration of 30g / L, hydrogen peroxide solution at 10g / L, sodium silicate solution at 10g / L, sodium carbonate solution at 10g / L and penetrant JFC-2 according to Mix the mass ratio of 2:2:2:2:1:1 to make a cooking liquid, put the washed flax fiber into the cooking liquid for degumming treatment, the cooking time is 60min, the cooking temperature is 70°C, the bath ratio The ratio is 1:15; hydrogen peroxide and alkali are used to act on flax fiber, and hydrogen pe...
Embodiment 3
[0027] (1) High temperature and high pressure pretreatment: The flax fiber is pretreated at a temperature of 105°C and a pressure of 0.4 atmospheres, and the treatment time is 30 minutes; the high temperature and high pressure pretreatment method is shorter than the ordinary acid-base pretreatment method. Less damage to fibers, resulting in low residual glue rate, high single fiber strength, effectively improving the quality of flax fibers,
[0028] (2 Washing: Washing the flax fiber pretreated by high temperature and high pressure at a temperature of 45°C;
[0029] (3) Chemical degumming treatment: Sodium hydroxide solution with mass concentration of 20g / L, hydrogen peroxide solution of 8g / L, sodium silicate solution of 8g / L, sodium carbonate solution of 8g / L and penetrant JFC-2 according to Mix the mass ratio of 2:2:2:2:1:1 to make a cooking liquid, put the washed flax fiber into the cooking liquid for degumming treatment, the cooking time is 70min, the cooking temperature i...
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