Colored curable composition, and color filter
A composition and hardening technology, applied in the field of color filters, can solve the problems of increased viscosity, poor dispersion stability, difficulty in further improving contrast and brightness, and achieve high contrast effects
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[0179] [Manufacturing Method of Colored Curable Composition]
[0180] The colored curable composition of the present invention is prepared by mixing the above-mentioned components and optional components as needed.
[0181] In addition, at the time of preparation of the curable colored composition, each component constituting the curable colored composition may be blended at one time, or may be blended sequentially after dissolving and dispersing each component in a solvent. In addition, there are no special restrictions on the input sequence or working conditions at the time of deployment. For example, the composition can be prepared by dissolving and dispersing all the components in a solvent at the same time, or if necessary, each component can be prepared in advance as two or more kinds of appropriate solutions and dispersions, and these solutions and dispersions can be mixed at the time of use (coating) Liquids are mixed to prepare compositions.
[0182] The colored cur...
example
[0250] Hereinafter, although an example demonstrates this invention more concretely, this invention is not limited to the following example unless the summary is exceeded. In addition, unless otherwise specified, "part" is a mass standard.
[0251] Exemplary compound Synthesis
[0252] A mixed solution of C.I. Pigment Green 7 (2.3 parts by weight), 4-dibutylaminocarbonylthiophenol (2.2 parts by weight), potassium carbonate (2.3 parts by weight), and NMP (methylpyrrolidone) (20 parts by weight) at 120 Stir at °C for 12 hours.
[0253] Ethyl acetate (50 parts by weight) and water (50 parts by weight) were added to the reaction liquid, and the water layer was neutralized with acetic acid.
[0254] After the organic layer was separated and concentrated, it was purified by silica gel chromatography to obtain 1.1 parts by weight of Exemplified Compound A-3.
[0255] The maximum absorption wavelength of the obtained compound in chloroform was 774 nm, and the molar absorpt...
example 1
[0314] The maximum absorption wavelength (λmax) in a chloroform solvent was measured for the phthalocyanine compound using an ultraviolet-visible spectrophotometer (UV2400-PC manufactured by Shimadzu Corporation). The measurement results are shown in the following tables.
[0315] [Table 1]
[0316] Exemplary compound
Maximum Absorption Wavelength (λmax)
molar absorptivity
A-1
730nm
100000
A-2
752nm
100000
A-3
774nm
115000
A-4
725nm
105000
A-5
740nm
115000
A-6
734nm
100000
A-7
708nm
130000
A-8
722nm
140000
A-9
728nm
135000
A-10
712nm
125000
A-11
705nm
145000
A-12
698nm
130000
A-13
700nm
135000
A-14
682nm
115000
A-15
691nm
125000
A-16
710nm
135000
A-17
725nm
145000
A-18
730nm
140000
A...
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