Thorium tungsten wire used for winding microwave oven magnetron and manufacturing method of thorium tungsten wire
A manufacturing method and magnetron technology, applied in the field of metal material manufacturing, can solve the problems of low creep resistance, easy brittle fracture, fast growth rate, etc. stable effect
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Embodiment 1
[0025] A method for manufacturing a thoriated tungsten wire for winding a microwave oven magnetron, comprising the following steps:
[0026] Step 1: Doping, mix and dry thorium nitrate solution, potassium nitrate solution, aluminum silicate solution and blue tungsten powder in the doping pot, and then send it to the reduction furnace.
[0027] Step 2: Reduction. The reduction furnace adopts a 5-stage temperature-controlled reduction process. The temperatures of the 4 stages are 550°C, 750°C, 850°C, and 950°C. / boat, the reducing atmosphere is hydrogen, and the flow rate of hydrogen is 3-5m 3 / h, reducing to obtain thoriated tungsten powder containing trace potassium elements, the powder particle size range is 1.3-1.5μm,
[0028] Step 3: High-energy ball milling, put the thoriated tungsten powder into a ball mill tank with polyurethane lining for high-energy ball milling for 3-5 hours, the ball milling medium is tungsten balls, the ball-to-material ratio is 5:1,
[0029] Ste...
Embodiment 2
[0037] A method for manufacturing a thoriated tungsten wire for winding a microwave oven magnetron, comprising the following steps:
[0038] Step 1: Doping, mix and dry the thorium nitrate solution, potassium nitrate solution, aluminum silicate solution and blue tungsten powder in the doping pot, then send them to the reduction furnace.
[0039] Step 2: Reduction, use 5-stage temperature-controlled reduction process to reduce the raw materials in the furnace, the 5-stage temperature is 550°C, 650°C, 750°C, 850°C, 950°C, and the holding time of each stage is 60-80min , the loading capacity is 300-350g / boat, the reducing atmosphere is hydrogen, and the flow rate of hydrogen is 3-5m 3 / h, reducing to obtain thoriated tungsten powder containing trace potassium elements, the powder fineness range is 1.3-1.5μm,
[0040] Step 3: High-energy ball milling, put the thoriated tungsten powder obtained in step 2 into a ball mill tank with polyurethane lining for high-energy ball milling f...
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