Preparation method of photonic crystal with inverse opal structure
An anti-opal structure and photonic crystal technology, applied in crystal growth, chemical instruments and methods, single crystal growth, etc., can solve the problems that colloids are difficult to fill gaps, opal structures are easy to fall off and destroy, and consume a lot of manpower, material resources and financial resources. , to achieve the effect of low cost, simple method and convenient operation
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[0034] Take 0.1 ml of 10% polystyrene microsphere suspoemulsion (weight percent, particle size: 330nm) and 0.05 ml of 10% TEOS aqueous solution (weight percent, expressed as SiO 2 Measure) into a 4ml cuvette, and add three milliliters of mill-Q water to the above cuvette, ultrasonically disperse for 10 minutes, and mix the above solution evenly. Then put a piece of clean glass substrate vertically into the above-mentioned cuvette. Put the cuvette on the heating stage, under the condition of 75 ℃, polystyrene microsphere template and SiO 2 The colloidal matrix was assembled and grown together on the glass substrate, kept warm for 48 hours, and taken out to obtain polystyrene microspheres and SiO 2 Colloidal composite structure. Put the above composite structure on a high-temperature heating table, heat it in air at 375 °C for 10 hours, and then take it out, thus obtaining high-quality, defect-free SiO 2 Inverse opal structure.
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