Method for drawing major-diameter optical fiber preform by continuous smelting furnace

A technology of optical fiber preform and continuous melting furnace, which is applied in the direction of manufacturing tools, glass molding, glass manufacturing equipment, etc., can solve the problems of high cost, making rods is not as good as buying rods, etc., and achieve low cost, strong competitiveness and cost reduction Effect

Inactive Publication Date: 2013-12-25
LIANYUNGANG HONGYANG QUARTZ PROD
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  • Abstract
  • Description
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Problems solved by technology

At present, there are more than 200 domestic optical cable manufacturers, most of whom rely on imported optical cables or optical fiber preforms to produce optical fiber products. In 2013, the domestic demand is expected to be about 2,500 tons, and the domestically produced preforms are about 1,250 tons. , the remaining 50% needs to be imported from abroad, the cost is high, resulting in the situation that making rods is not as good as buying rods

Method used

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  • Method for drawing major-diameter optical fiber preform by continuous smelting furnace

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Embodiment Construction

[0015] A method for drawing a large-diameter optical fiber preform with a furnace,

[0016] (1) Preparation of high-purity quartz sand

[0017] First, raw silica (SiO 2 ) to remove the sediment and impurities on the surface with water; mechanically crush until the diameter of the pieces is not greater than 25mm; then soak in the mixed acid reaction tank for 48 hours, and then wash the acid solution with water; enter the roasting, the roasting temperature is 1100 ° C ± 10 ° C , roasted for 2 hours, and kept at constant temperature for one hour; then take out the calcined quartz stone and put it in cold water to quench it, change the crystal structure of the quartz stone, use deionized water, the conductivity is -6 , water temperature <15°C; dry the quenched quartz stone at a temperature of 500°C; then enter the pulverizer to be crushed into quartz sand with a particle size of 0.25-0.15mm; then enter the strong magnetic field to remove iron; then the quartz sand Sorting (40 me...

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Abstract

The invention discloses a method for drawing a major-diameter optical fiber preform by a continuous smelting furnace. The method comprises the steps that high-purity quartz sand is prepared firstly; raw silica is subjected to water washing, crushing, pickling, roasting, water quenching, drying, smashing, iron removal, sorting and floatation sequentially; the quartz sand is put into a reaction kettle; mixed acid is added, and reacts for over 24h while rotation is performed; the high-purity quartz sand in the reaction kettle is taken out and dried for standby application; a core bar in the continuous smelting furnace is dismounted; a forming device is arranged below a material platform outlet at the bottom of a tungsten crucible, wherein the forming device comprises a stand pipe butted with the material platform outlet; a horn-mouth-shaped opening protector is arranged at the lower end of the stand pipe; a smooth necking section is arranged at the bottom of a material platform, and butted with an upper port of the stand pipe; a computer system and a laser diameter measurement system are combined for control; and the satisfactory major-diameter optical fiber preform is drawn. According to the method, a finished product rate of the major-diameter high-purity optical fiber preform is greater than or equal to 90%, a hydroxyl value is less than or equal to 1ppm, and the content of SiO2 reaches 99.9999%.

Description

technical field [0001] The invention relates to a quartz product, in particular to a method for drawing a large-diameter optical fiber preform with a melting furnace. Background technique [0002] Optical fiber quartz preform has the characteristics of higher purity, high tensile strength, and high optical stability. It has a large market demand and is suitable for military, civil, aviation and other communication (communication) fields. At present, there are only general diameters of a few millimeters to tens of millimeters (called light rods) on the market. The commonly used manufacturing processes are external vapor deposition method OVD, vapor phase axial deposition method VAD, improved vapor deposition method MCVD and plasma chemical vapor deposition process PVCD. and other mixing processes. At present, there are more than 200 domestic optical cable manufacturers, most of whom rely on imported optical cables or optical fiber preforms to produce optical fiber products....

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C03B20/00C03B37/012
CPCC03B37/01274C03B2205/04
Inventor 徐传龙冯维娥徐源
Owner LIANYUNGANG HONGYANG QUARTZ PROD
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