Light-reflection, heat-insulation and anticorrosion paint and preparation method thereof
An anti-corrosion coating and light reflection technology, applied in anti-corrosion coatings, reflection/signal coatings, coatings, etc., can solve problems such as mold growth, and achieve the effects of prolonging service life, good heat insulation performance, and good weather resistance
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Embodiment 1
[0026] A method for preparing a light-reflecting heat-insulating anti-corrosion coating of the present invention is prepared by the following steps:
[0027] (1) Preparation of nano-titanium dioxide-coated hollow glass microspheres
[0028] Wash the hollow glass microspheres several times with distilled water and absolute ethanol to make the hollow glass microspheres form a hydrophilic surface, add 5g of hollow glass microspheres after cleaning to 50g of distilled water, and place them in a constant temperature water bath at 55°C with a homogeneous The disperser was stirred at a low speed of 200 rev / m for 10 minutes, and at the same time, 5ml of 1% sodium dodecylbenzenesulfonate solution was added dropwise, heated to 80°C, and 0.1mol / l Ti(SO 4 ) 2 solution, while slowly adding 0.1mol / l NaOH solution dropwise to maintain pH = 3.0 ~ 3.5, after about 5 hours the hydrolysis reaction ends, suction filtration and washing until pH = 7, the prepared hollow glass microspheres / TiO 2 T...
Embodiment 2
[0040] A method for preparing a light-reflecting heat-insulating anti-corrosion coating of the present invention is prepared by the following steps:
[0041] (1) Preparation of nano-titanium dioxide-coated hollow glass microspheres
[0042] Wash the hollow glass microspheres several times with distilled water and absolute ethanol to make the hollow glass microspheres form a hydrophilic surface, add 5g of hollow glass microspheres after cleaning to 50g of distilled water, and place them in a constant temperature water bath at 55°C with a homogeneous The disperser was stirred at a low speed of 200 rev / m for 10 minutes, and at the same time, 5ml of 1% sodium dodecylbenzenesulfonate solution was added dropwise, heated to 80°C, and 0.1mol / l Ti(SO 4 ) 2 solution, while slowly adding 0.1mol / l NaOH solution dropwise to maintain pH = 3.0 ~ 3.5, after about 5 hours the hydrolysis reaction ends, suction filtration and washing until pH = 7, the prepared hollow glass microspheres / TiO 2 T...
Embodiment 3
[0054] (1) Hollow glass microspheres coated with nano-titanium dioxide
[0055] Wash the hollow glass microspheres several times with distilled water and absolute ethanol to make the hollow glass microspheres form a hydrophilic surface, add 5g of hollow glass microspheres after cleaning to 50g of distilled water, and place them in a constant temperature water bath at 55°C with a homogeneous The disperser was stirred at a low speed of 200 rev / m for 10 minutes, and at the same time, 5ml of 1% sodium dodecylbenzenesulfonate solution was added dropwise, heated to 80°C, and 0.1mol / l Ti(SO 4 ) 2 solution, while slowly adding 0.1mol / l NaOH solution dropwise to maintain pH = 3.0 ~ 3.5, after about 5 hours the hydrolysis reaction ends, suction filtration and washing until pH = 7, the prepared hollow glass microspheres / TiO 2 The complex was dried at 120° C. for 2 hours, and then calcined in a muffle furnace at 600° C. for 2 hours to prepare nano-titanium dioxide-coated hollow glass mic...
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