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Low-noise lubricating grease and preparation method and application thereof

A lubricating grease and low-noise technology, which is applied in the field of low-noise lubricating grease and its preparation, can solve the problems of unfavorable development and promotion of low-noise lubricating grease, high price, complicated production process, etc.

Active Publication Date: 2014-03-12
XINXIANG HENGXING TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

For example, this kind of low-noise grease has been more widely used in sports machinery with high motion precision, high speed and long oil change intervals, especially in micro-mechanical bearings with high motion precision and noise requirements, but at present The low-noise lubricating grease used in my country has the following problems: one, low-noise lubricating grease is used as high-grade lubricating grease, and the import price is often more expensive, which is not conducive to the development and promotion of low-noise lubricating grease; The production process of lubricating grease for low-precision and low-noise miniature bearings is relatively complicated, the production cost is relatively high, and the product performance is unstable. The motion accuracy of miniature bearings, meanwhile, increases wear and vibration, resulting in greater motion noise

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] (1) Add 12 parts by weight of lauryl hydroxystearic acid and 25 parts by weight of mineral oil into the saponification kettle, gradually raise the temperature and start stirring after the fatty acid is dissolved;

[0026] (2) Dissolve 5 parts by weight of lithium hydroxide in water to form an aqueous solution of lithium hydroxide. When the temperature of the mixed solution in step (1) rises to 50-60°C, add the aqueous solution of lithium hydroxide to the saponification kettle middle;

[0027] (3) Dilute 2.5 parts by weight of boric acid with water of 4 times the mass of boric acid, and heat to 95°C to form a hot aqueous solution of boric acid. Stir the mixed solution in step (2) for 20 min, then add the hot aqueous solution of boric acid, and continue heating at Saponification at 90-92°C for 2-4 hours;

[0028] (4) After the saponification reaction is completed, continue to stir and raise the temperature for dehydration. When the temperature reaches 150-160°C, add 45 p...

Embodiment 2

[0031] (1) Add 15 parts by weight of stearic hydroxy fatty acid and 20 parts by weight of olefin oil into the saponification kettle, gradually raise the temperature and start stirring after the fatty acid is dissolved;

[0032] (2) Dissolve 2 parts by weight of lithium hydroxide in water to form an aqueous solution of lithium hydroxide. When the temperature of the mixed solution in step (1) rises to 50-60°C, add the aqueous solution of lithium hydroxide to the saponification kettle middle;

[0033] (3) Dilute 5 parts by weight of boric acid with water of 4 times the mass of boric acid, and heat to 95°C to form a hot water solution of boric acid. Stir the mixed solution in step (2) for 20 min, then add the hot water solution of boric acid, and continue heating at Saponification at 90-92°C for 2-4 hours;

[0034] (4) After the saponification reaction is completed, continue to stir and raise the temperature for dehydration. When the temperature reaches 150-160°C, add 45 parts by...

Embodiment 3

[0037] (1) Add 10 parts by weight of behenic acid and 35 parts by weight of silicone oil into the saponification kettle, gradually raise the temperature until the fatty acid is dissolved, and then start stirring;

[0038](2) Dissolve 8 parts by weight of lithium hydroxide in water to form an aqueous solution of lithium hydroxide. When the temperature of the mixed solution in step (1) rises to 50-60°C, add the aqueous solution of lithium hydroxide to the saponification kettle middle;

[0039] (3) Dilute 1 part by weight of boric acid with water 4 times the mass of boric acid, and heat it to 95°C to form a hot water solution of boric acid. Stir the mixed solution in step (2) for 20 min, then add the hot water solution of boric acid, and continue heating at Saponification at 90-92°C for 2-4 hours;

[0040] (4) After the saponification reaction is completed, continue to stir and raise the temperature for dehydration. When the temperature reaches 150-160°C, add 50 parts by weight ...

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PUM

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Abstract

The invention discloses low-noise lubricating grease and a preparation method and application thereof. The invention adopts the technical scheme as follows: the low-noise lubricating grease is prepared from the raw materials in parts by weight: 65-85 parts of base oil, 10-15 parts of C12-C22 hydroxy fatty acid, 2-8 parts of lithium hydroxide (LiOH.H2O), 1-5 parts of boric acid, m parts of dimethyl terephthalate (m is greater than or equal to 0, but smaller than or equal to 1), n parts of benzoic acid (n is greater than or equal to 0, but smaller than or equal to 2), 1-3 parts of antioxidant and 1-3 parts of sulfosalicylic acid. The invention further discloses the preparation method of the low-noise lubricating grease and application of the low-noise lubricating grease to high-precision miniature mechanical bearings. The low-noise lubricating grease is reasonable in formulation, and relatively high in production efficiency; after the low-noise lubricating grease is ground by a grinder, which is a patented product of the Company, the particle sizes of mechanical impurities in the low-noise lubricating grease are controlled to be smaller than those of mechanical impurities in the exhibiting lubricating grease, and the vibrating decibel value of a bearing lubricated by the low-noise lubricating grease is lower than that of a bearing lubricated by the exhibiting lubricating grease, thus ensuring the running accuracy of the miniature bearing and reducing vibration and abrasion; the vibrating decibel value of the bearing is lower than 40 decibels; and the particle sizes of the mechanical impurities in the low-noise lubricating grease are smaller than 2 microns.

Description

technical field [0001] The invention relates to the field of lubricating grease for high-precision micro-mechanical bearings, in particular to a low-noise lubricating grease and a preparation method and application thereof. Background technique [0002] With the development of the economy, mechanical equipment puts forward higher requirements for lubricating grease. In many technical fields, ultra-pure and low-noise lubricating grease is required in order to reduce the noise value of rolling bearings and the acoustic emission in the air. It meets the noise limits and tight running tolerances of precision rolling bearings and guarantees economical and energy-saving operation. For example, this kind of low-noise grease has been more widely used in sports machinery with high motion precision, high speed and long oil change interval, especially in micro-mechanical bearings with high motion precision and noise requirements, but at present The low-noise lubricating grease used...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C10M169/00C10M177/00C10N40/02
Inventor 周忠太朱命阳郭培伟时红敏张雪
Owner XINXIANG HENGXING TECH CO LTD
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