Low-noise lubricating grease and preparation method and application thereof
A lubricating grease and low-noise technology, which is applied in the field of low-noise lubricating grease and its preparation, can solve the problems of unfavorable development and promotion of low-noise lubricating grease, high price, complicated production process, etc.
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Embodiment 1
[0025] (1) Add 12 parts by weight of lauryl hydroxystearic acid and 25 parts by weight of mineral oil into the saponification kettle, gradually raise the temperature and start stirring after the fatty acid is dissolved;
[0026] (2) Dissolve 5 parts by weight of lithium hydroxide in water to form an aqueous solution of lithium hydroxide. When the temperature of the mixed solution in step (1) rises to 50-60°C, add the aqueous solution of lithium hydroxide to the saponification kettle middle;
[0027] (3) Dilute 2.5 parts by weight of boric acid with water of 4 times the mass of boric acid, and heat to 95°C to form a hot aqueous solution of boric acid. Stir the mixed solution in step (2) for 20 min, then add the hot aqueous solution of boric acid, and continue heating at Saponification at 90-92°C for 2-4 hours;
[0028] (4) After the saponification reaction is completed, continue to stir and raise the temperature for dehydration. When the temperature reaches 150-160°C, add 45 p...
Embodiment 2
[0031] (1) Add 15 parts by weight of stearic hydroxy fatty acid and 20 parts by weight of olefin oil into the saponification kettle, gradually raise the temperature and start stirring after the fatty acid is dissolved;
[0032] (2) Dissolve 2 parts by weight of lithium hydroxide in water to form an aqueous solution of lithium hydroxide. When the temperature of the mixed solution in step (1) rises to 50-60°C, add the aqueous solution of lithium hydroxide to the saponification kettle middle;
[0033] (3) Dilute 5 parts by weight of boric acid with water of 4 times the mass of boric acid, and heat to 95°C to form a hot water solution of boric acid. Stir the mixed solution in step (2) for 20 min, then add the hot water solution of boric acid, and continue heating at Saponification at 90-92°C for 2-4 hours;
[0034] (4) After the saponification reaction is completed, continue to stir and raise the temperature for dehydration. When the temperature reaches 150-160°C, add 45 parts by...
Embodiment 3
[0037] (1) Add 10 parts by weight of behenic acid and 35 parts by weight of silicone oil into the saponification kettle, gradually raise the temperature until the fatty acid is dissolved, and then start stirring;
[0038](2) Dissolve 8 parts by weight of lithium hydroxide in water to form an aqueous solution of lithium hydroxide. When the temperature of the mixed solution in step (1) rises to 50-60°C, add the aqueous solution of lithium hydroxide to the saponification kettle middle;
[0039] (3) Dilute 1 part by weight of boric acid with water 4 times the mass of boric acid, and heat it to 95°C to form a hot water solution of boric acid. Stir the mixed solution in step (2) for 20 min, then add the hot water solution of boric acid, and continue heating at Saponification at 90-92°C for 2-4 hours;
[0040] (4) After the saponification reaction is completed, continue to stir and raise the temperature for dehydration. When the temperature reaches 150-160°C, add 50 parts by weight ...
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