Powder granulating method
A powder and granulation technology, applied in the field of powder metallurgy, can solve the problems of material pollution and achieve the effect of ensuring uniformity
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Embodiment 1
[0013] Embodiment one: a kind of method of silver carbon (AgC4) powder granulation, the electrolytic silver powder (-300 order) of 96% (weight percent) is mixed with the graphite (average particle diameter 1 μ m) of 4%, mix powder in Press it into a compact in the mold (compressed relative density is about 80%), crush the compact into granules with a particle size of 0.2-0.6mm, put the granules into an inert atmosphere sintering furnace at 550°C for sintering, and hold the time After 2 hours, cool to room temperature and take it out. The sintered granules are crushed in a pulverizer, and then passed through a sieve of 80 mesh and 320 mesh. It is required to continue pressing, crushing, sintering, crushing, and sieving until the obtained powder has good fluidity and uniform composition.
Embodiment 2
[0014] Embodiment two: [0010] a kind of silver tin oxide [AgSnO2 (12)] powder granulation method, the silver tin oxide of co-precipitation is mixed, mixed powder is pressed into compact in mold (compression relative density is about 75%), crush the agglomerate into granules with a particle size of 0.2-0.6 mm, put the granules into a sintering furnace with an oxidizing atmosphere and sinter at 600 ° C, hold for 2 hours, cool to room temperature, take out, and the sintered granules The granules are crushed in the pulverizer, and then passed through 80 mesh sieve and 320 mesh sieve, the powder on the 80 mesh sieve continues to be crushed, and the powder below 320 mesh is re-granulated, that is, the pressing, crushing, sintering, crushing, and passing are continued according to the above requirements. Sieve until the obtained powder has good fluidity and uniform composition.
Embodiment 3
[0015] Embodiment three: a kind of method of silver tungsten [AgW (50)] powder granulation, with the electrolytic silver powder (-300 order) of 50% (weight percentage) and the tungsten powder (average particle diameter 5 μ m) of 50% (weight percentage) ) for mixing, the mixed powder is pressed into a compact in a mold (compressed relative density is about 60%), the compact is crushed into granules with a particle size of 0.2-0.6mm, and the granules are put into a sintering furnace with an inert atmosphere Sinter at 750°C, hold for 2 hours, cool to room temperature and take it out. The sintered particles are crushed in the pulverizer, and then pass through 80 mesh sieve and 320 mesh sieve. The powder on the 80 mesh sieve continues to be crushed. Re-granulate, that is, continue to press, pulverize, sinter, pulverize, and sieve according to the above requirements until the obtained powder has good fluidity and uniform composition.
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Abstract
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