Novel corrosion and scale inhibitor and preparation method thereof
A technology of corrosion and scale inhibitor, corrosion inhibitor, applied in chemical instruments and methods, descaling and water softening, water/sludge/sewage treatment, etc. Efficiency, pipe string corrosion and other issues, to achieve the effect of preventing scaling
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Embodiment 1
[0022] This example provides a new type of corrosion and scale inhibitor, which contains corrosion inhibitor, scale inhibitor and hydroxyethylidene diphosphonic acid in a mass ratio of 0.5:80:10.
[0023] The preparation method of above-mentioned novel corrosion and scale inhibitor specifically comprises the following steps:
[0024] 1, the preparation of corrosion inhibitor, it may further comprise the steps:
[0025] Step 1: Slowly add diethylenetriamine to the uniformly dissolved oleic acid containing 10mL water-carrying agent and 0.5g zeolite, the molar ratio of oleic acid and diethylenetriamine is 1:1.1, stir at 160°C, and carry out 2h acylation reaction, then heated up to 220°C, stirred, and cyclization reaction was carried out for 6h to obtain the imidazoline intermediate;
[0026] Step 2: Cool the imidazoline intermediate to 70°C, stir, add a quaternization reagent to the imidazoline intermediate, the molar ratio of the imidazoline intermediate to the quaternization r...
Embodiment 2
[0037] This example is based on the novel corrosion and scale inhibitor described in Example 1 and its preparation method. Corrosion inhibitors, scale inhibitors and Hydroxyethylidene diphosphonic acid, the preparation steps given in Example 1 were carried out under the same conditions to prepare a new type of corrosion and scale inhibitor, as the control group 1 and control group 2 of Example 1.
Embodiment 3
[0039] The new corrosion and scale inhibitors prepared in Example 1, control group 1 and control group 2 were evaluated for their corrosion and scale inhibition performance.
[0040] Corrosion inhibitor performance evaluation
[0041] Referring to the Petroleum and Natural Gas Industry Standard of the People's Republic of China SY / T5273-2000 "Evaluation Method for the Performance of Corrosion Inhibitors for Oilfield Produced Water", the new corrosion and scale inhibitors prepared in Example 1, Control Group 1 and Control Group 2 were tested by the classic weight loss method Evaluation of corrosion inhibition performance.
[0042] The experimental method includes the following steps:
[0043] Prepare the formation water samples of the simulated oil production site. Under the conditions of normal pressure and 45°C constant temperature, put the previously treated test piece (N80 steel piece) into the constant temperature formation water sample solution to be tested. The amount o...
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