Antibacterial PPR pipe
A technology for pipes and antibacterial agents, applied in the field of antibacterial PPR pipes, can solve the problems of complex process and long reaction time, and achieve the effects of simple preparation process, low cost and cost reduction.
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Embodiment 1
[0027] (1) Preparation of silica-loaded nano-silver antibacterial agent
[0028] Stir 0.01g of silver nitrate, 50ml of tetraethyl orthosilicate, 400ml of absolute ethanol and 40ml of ammonia water at 35°C for 4 hours at a constant temperature; filter the obtained product, wash with water, and dry to obtain a silica powder that adsorbs silver ammonium ions. Disperse the silica powder adsorbed with silver ammonium ions in water, add a sodium borohydride aqueous solution with a concentration of 0.01 g / mL dropwise at a rate of 0.042 mL / min for 60 minutes, and prepare silica-loaded nano Silver antibacterial agent suspension; then filter the obtained silicon dioxide-loaded nano-silver antibacterial agent suspension, wash with water, and dry to obtain silicon dioxide-loaded nano-silver antibacterial agent powder.
[0029] (2) Preparation of antibacterial PPR pipe
[0030] After the silica-loaded nano-silver antibacterial agent with a weight of 2% of all components is treated with a ...
Embodiment 2
[0033] (1) Preparation of silica-loaded nano-silver antibacterial agent
[0034] Stir 0.06g of silver nitrate, 60ml of tetraethyl orthosilicate, 400ml of absolute ethanol and 40ml of ammonia water at a constant temperature of 35°C for 5h; filter the obtained product, wash it with water, and dry it to obtain a silica powder that adsorbs silver ammonium ions. Disperse the silica powder adsorbed with silver ammonium ions in water, add a sodium borohydride aqueous solution with a concentration of 0.02 g / mL dropwise at a rate of 0.1 mL / min for 30 min, and prepare silica-loaded nanoparticles. Silver antibacterial agent suspension; then filter the obtained silicon dioxide-loaded nano-silver antibacterial agent suspension, wash with water, and dry to obtain silicon dioxide-loaded nano-silver antibacterial agent powder.
[0035] (2) Preparation of antibacterial PPR pipe
[0036] After the silica-loaded nano-silver antibacterial agent with a weight of 1.8% of all components is trea...
Embodiment 3
[0039] (1) Preparation of silica-loaded nano-silver antibacterial agent
[0040] Stir 0.12g of silver nitrate, 60ml of tetraethyl orthosilicate, 450ml of absolute ethanol and 45ml of ammonia water at 35°C for 6 hours at a constant temperature; filter the obtained product, wash it with water, and dry it to obtain a silica powder that adsorbs silver ammonium ions. Disperse the silica powder adsorbed with silver ammonium ions in water, add a sodium borohydride aqueous solution with a concentration of 0.01 g / mL dropwise at a rate of 1 mL / min for 40 min, and prepare silica-loaded nano-silver Antibacterial agent suspension; then filter the obtained silicon dioxide-loaded nano-silver antibacterial agent suspension, wash with water, and dry to obtain silicon dioxide-loaded nano-silver antibacterial agent powder.
[0041] (2) Preparation of antibacterial PPR pipe
[0042]After the silica-loaded nano-silver antibacterial agent with a weight of 1.5% of all components is treated with...
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