A kind of preparation method of hydrogenation catalyst
A technology of hydrogenation catalyst and pore-enlarging agent, which is applied in the field of hydrogenation catalyst preparation, can solve problems such as uneven distribution of active metal components, influence on catalyst performance, and poor catalyst strength, so as to prevent dust pollution and harm people Harm, shorten drying time, low cost effect
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Embodiment 1
[0021] 2L sodium metaaluminate aqueous solution (with Al 2 o 3 The concentration is 15g / 100mL) and 3L aluminum sulfate aqueous solution (as Al 2 o 3 The concentration of the meter is 3g / 100mL) and put them into the container at the high position respectively, and the flow meter flows into the stainless steel container equipped with a 6L clean water belt agitator and a heating mantle, and heats to 60°C; Aluminum sulfate solution, reduce the pH value of the slurry to 3.0, and after stabilizing for 10 minutes, add the two materials into the stainless steel tank at a certain speed at the same time, keep the pH value at 7.3, and neutralize the gelling reaction for 15 minutes. Then stop adding aluminum sulfate solution, so that the pH value rises to 9.2, stop adding sodium metaaluminate solution, and stabilize for a period of time; pass through aluminum sulfate solution, reduce the pH value of the slurry to 3.0, and stabilize for a period of time; pass through sodium metaaluminate...
Embodiment 2
[0023] Compared with Example 1, after the slurry was filtered and washed, it was dried at 110° C. for 1 hour to obtain pseudo-boehmite with a dry basis of 50%. Weighed 200 grams of pseudo-boehmite and 5.0 grams of carbon black , 2.0 grams of extrusion aid squash powder and 80ml of active metal salt solution, containing ammonium molybdate and basic nickel carbonate in the active metal salt solution, the content is based on MoO 3 15 wt% as NiO, and 3 wt% as NiO. Other material consumption and operating conditions are identical with embodiment 1, make catalyst B.
Embodiment 3
[0025] Compared with Example 1, the slurry was filtered, washed, and dried at 100° C. for 1 hour to obtain pseudo-boehmite with a dry basis of 40%. Other material consumption and operating conditions are identical with embodiment 1, make catalyst C.
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