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Use of isopropyl acetate as leaching solvent in leaching vegetable oil and method for leaching oil using it

A technology of isopropyl acetate and vegetable oil, which is applied in the direction of fat oil/fat production and fat generation, can solve the problems of insufficient attention to toxicity, lack of understanding, and large loss of ethanol solvent, so as to achieve stable supply and quality, prolong service life, The effect of increasing business efficiency

Active Publication Date: 2015-08-19
HUNAN ZHONGCHUANG CHEM
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the vegetable oil extraction solvent has the following defects: 1) The flash point of the vegetable oil extraction solvent is low (the flash point of n-hexane is below -23°C, the flash point of cyclohexane is -17°C, and the flash point of other C6 alkanes is -6 below ℃), it is more dangerous during storage and use
2) Vegetable oil extraction solvents are highly volatile and highly fat-soluble. In particular, n-hexane can accumulate in the human body and is highly toxic to the nervous system. Due to lack of protection, insufficient attention or lack of understanding of its toxicity, n-hexane has appeared in many places Poisoning tragedies (such as the poisoning of Apple supplier workers)
In particular, aromatic solvents such as benzene remain in the vegetable oil extraction solvent, which is more toxic
3) Vegetable oil extraction solvent contains corrosive impurities such as sulfur, which is highly corrosive to the system
4) The composition of the vegetable oil extraction solvent is unstable, and each factory and batch has a great influence, which makes the extraction process change greatly
Although supercritical fluid extraction of vegetable oil has obvious advantages, it is difficult to apply it on a large scale because of its high requirements for equipment.
Ethanol, oilseed meal has a strong adsorption effect on ethanol, the loss of ethanol solvent is relatively large, the industrialization cost is too high, and the leaching of water-containing ethanol will make the leached oil contain more sugars, proteins and other colloids, which will cause harm to the process operation

Method used

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  • Use of isopropyl acetate as leaching solvent in leaching vegetable oil and method for leaching oil using it

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0055] Example 1 (comparative example)

[0056] Soybean is selected as the oil, and the vegetable oil extraction solvent is the extraction solvent to extract soybean oil. The process is as follows:

[0057] The raw soybeans are cleaned, dried, crushed and peeled, and then heated to 78°C to soften and bind the billet. The thickness of the billet is about 0.3mm; the prepared billet is leached in a flat rotary extractor with vegetable oil extraction solvent , The solvent and the material embryo are in countercurrent contact with immersion and spray mixing. The ratio of the leaching solvent to the oil is 0.8:1 by weight; the leaching time is 60min; the temperature is 78℃, filtered and separated to obtain 30wt% mixed oil and solvent content It is 35wt% wet meal. A high-temperature desolventization process is used to desolve the wet meal, and the residual oil content of the meal is about 0.8wt% after the desolventizing process. Pass the mixed oil into an evaporator for evaporation, the...

Embodiment 2

[0059] Soybean is used as oil and isopropyl acetate is used as extraction solvent to extract soybean oil. The process is as follows:

[0060] The raw soybeans are cleaned, dried, crushed and peeled, and then heated to 78°C to soften and roll the billet. The thickness of the billet is about 0.3mm; the prepared billet is leached in a flat-rotating extractor with isopropyl acetate , The solvent and the raw material are contacted by immersion, spray mixing and countercurrent flow. The ratio of the leaching solvent to the oil is 0.8:1 by weight; the leaching time is 60min; the temperature is 78℃, filtered and separated to obtain 48wt% mixed oil and solvent content It is 30wt% wet meal. A high-temperature desolventization process is used to desolve the wet meal, and the residual oil content of the meal after desolventizing is about 0.6wt%. The mixed oil is passed into an evaporator for evaporation, the outlet solvent gas temperature is 88°C; the once-evaporated mixed oil is re-evapora...

Embodiment 3

[0062] Using peanut as the oil and isopropyl acetate as the extraction solvent to extract peanut oil, the process is as follows:

[0063] The raw peanuts are cleaned, dried, crushed and peeled, and then heated to 74°C to soften and roll the billet. The thickness of the billet is about 0.3mm; then the oil billet is heated to 120°C for extruding and puffing, and it is heated by a dryer. Dry the preform to 3% moisture at 75°C; use isopropyl acetate to leaching the prepared preform in a flat-rotation extractor. The solvent and the preform are in countercurrent contact with immersion and spray mixing. The oil-to-feed ratio is 0.4:1 by weight; the leaching time is 80min; the temperature is 85°C to obtain 49% mixed oil and 25% solvent content wet meal. A high-temperature desolventization process is used to desolve the wet meal, and the residual oil content of the meal after desolventizing is about 0.6wt%. The mixed oil is passed into an evaporator for evaporation, the outlet solvent ga...

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Abstract

The invention discloses use of isopropyl acetate as a leaching solvent in plant oil and fat leaching and an oil and fat leaching method using the isopropyl acetate. The method is as follows: 1) crushing a plant oil and fat raw material to obtain a crushed matter or pre treating the plant oil and fat raw material to obtain a blank sheet or pre pressing the plant oil and fat raw material to obtain a pressed cake; 2) using the isopropyl acetate to leach the crushed matter or the pressed cake obtained by the step 1), then performing solid-liquid separation to obtain mixed oil and wet meal; 3) separating the mixed oil leached by the step 2) to obtain plant oil and fat. The method uses the isopropyl acetate which can be used as an edible spice as a solvent, the leached oil and fat is free of sulfur and benzene, the high concentration and high quality oil and fat is obtained, and the process can improve the leaching efficiency and reduce energy consumption.

Description

Technical field [0001] The invention belongs to the technical field of vegetable oil extraction, and specifically relates to the use of isopropyl acetate as a leaching solvent for leaching vegetable oils and a method for extracting oils using the same. Background technique [0002] In the production process of vegetable fats and oils, the leaching method is a more advanced oil-making method. It applies the principle of solid-liquid extraction, selects an organic solvent that can dissolve the fat, and contacts the oil (soaking or spraying) , A method of extracting the fat in the oil, mostly using pre-pressed cake and then leaching. The leaching method has the advantages of high oil yield, low residual oil rate in meal, low labor intensity, high production efficiency, low protein denaturation in meal, good quality, and easy realization of large-scale production and production automation. [0003] In my country, the use of direct leaching or pre-pressing leaching process of vegetable...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C11B1/10C11B1/00
Inventor 胡先念刘粮帅叶文
Owner HUNAN ZHONGCHUANG CHEM
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