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Preparation method of catalyst in combustor of micro-methanol reformer

A technology of reformer and combustion chamber, applied in chemical instruments and methods, physical/chemical process catalysts, metal/metal oxide/metal hydroxide catalysts, etc., can solve the problem of small contact area between reaction gas and catalyst, catalyst adhesion Focus on problems such as poor strength and low catalyst utilization rate, and achieve the effects of low cost, extended service life, and improved stability

Active Publication Date: 2016-03-16
HARBIN INST OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The catalyst prepared by the invention can effectively solve the problems of poor adhesion of the catalyst, small contact area between the reaction gas and the catalyst, and low utilization rate of the catalyst in the combustion chamber of the existing methanol reformer.

Method used

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  • Preparation method of catalyst in combustor of micro-methanol reformer
  • Preparation method of catalyst in combustor of micro-methanol reformer

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] The combustion chamber of the miniature methanol reformer is made of aluminum alloy, and its composition includes an aluminum alloy body, an aluminum alloy package end plate and a flow field structure. The flow field structure is used as a gas circulation channel in the combustion chamber, located between the aluminum Between the end plates of the alloy package, on the surface of the aluminum alloy body. A layer of plexiglass is covered on the surface of the aluminum alloy body with flow channels and the flow channels are exposed, and then placed in such figure 1 In the electrolytic cell shown, the electrolytic cell is used as the cathode and the aluminum alloy body is used as the anode to perform micro-arc oxidation treatment on the flow channel. Among them: the electrolyte is a mixed solution of 5-15g / L sodium aluminate and 0.5-2.0g / L sodium hypophosphite, and the DC power supply provides an output voltage range between 400-700V, using 5-20A / dm 2 The current density ...

Embodiment 2

[0024] The difference between this example and Example 1 is that the electrolyte is a mixed solution of 10g / L sodium aluminate and 1.0g / L sodium hypophosphite, the output voltage provided by the DC power supply is 300V, and the current density is 15A / dm 2 , with a processing time of 60 minutes.

Embodiment 4

[0026] The difference between this embodiment and Embodiment 1 is that the micro-arc oxidation power supply is a bidirectional pulse power supply, and the positive pulse voltage is 400-600V, the negative pulse voltage is 0-300V, and the pulse frequency is 10-5000Hz. -120 minutes.

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Abstract

The invention discloses a method for preparing a catalyst for a combustion chamber of a micro-methanol reformer. The steps of the method are as follows: the combustion chamber of the reformer with a flow field is used as an anode, placed in an electrolyte, and a DC or AC voltage is applied to the catalyst. The flow field is processed to form a layer of porous oxide ceramic film on the surface of the flow field, and then use it as a carrier to load the reforming catalyst Pt. The present invention adopts the micro-arc oxidation technology to directly grow the oxide ceramic film containing Al2O3 in situ on the surface of the flow field, and then use it as a carrier to deposit Pt. The catalyst prepared by the present invention can effectively solve the problem of existing methanol reformer combustion chamber There are problems such as poor adhesion of the catalyst, small contact area between the reaction gas and the catalyst, and low utilization of the catalyst.

Description

technical field [0001] The invention belongs to the technical field of proton exchange membrane fuel cell fuel, and relates to a method for preparing a catalyst used in a combustion chamber of a methanol reformer. Background technique [0002] There are two major problems in the utilization of traditional energy that plague people. One is that mechanical energy or electrical energy must be output through processes such as combustion, but limited by the Carnot cycle, the energy conversion rate is only 33-35%, and nearly 60% of the energy is lost during this transformation process; the second is that energy is being used The process has caused a lot of waste gas, waste water, waste residue, waste heat and noise pollution to the living environment. Over the years, countries have been trying to find energy utilization methods that can efficiently utilize energy without polluting the environment. Clean and efficient fuel cell technology has gradually entered the field of vision ...

Claims

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Application Information

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IPC IPC(8): B01J23/42H01M4/92
CPCY02E60/50
Inventor 张雪林刘晓为陈海龙张宇峰
Owner HARBIN INST OF TECH
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